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The application of 1H/13C inversely correlated NMR spectroscopy to the determination of acylation and glycosylation sites in the O-specific polysaccharide from Hafnia alvei 1187.

作者信息

Dabrowski J, Hauck M, Romanowska E, Gamian A

出版信息

Biochem Biophys Res Commun. 1987 Aug 14;146(3):1283-5. doi: 10.1016/0006-291x(87)90787-x.

DOI:10.1016/0006-291x(87)90787-x
PMID:3619933
Abstract

An inversely correlated 1H/13C NMR spectrum defined the amino sugars acylated by acetyl or 3-hydroxybutyryl groups and revealed partial sequences and glycosylation sites in a tetrasaccharide repeating unit of the title polysaccharide, (----2DGlc alpha 1----3DGlcNAcyl alpha 1----4DGalNAc alpha 1----3DGalNAc beta 1----)n, where Acyl = 3-hydroxybutyryl.

摘要

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