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水热降解对各种含立方相半透明氧化锆弯曲疲劳强度的影响

Effect of Hydrothermal Degradation on Flexural Fatigue Strength of Various Cubic-Containing Translucent Zirconia.

作者信息

Kengtanyakich Santiphab, Peampring Chaimongkon

机构信息

Department of Prosthetic Dentistry, Faculty of Dentistry, Prince of Songkla University, Songkhla, Thailand.

出版信息

Eur J Dent. 2023 Jul;17(3):777-783. doi: 10.1055/s-0042-1755630. Epub 2022 Oct 11.

Abstract

OBJECTIVE

The aim of this study is to investigate the fatigue and hydrothermal degradation behavior among the cubic-containing translucent yttrium oxide stabilized tetragonal zirconia polycrystal (Y-TZP).

MATERIALS AND METHODS

Four groups of commercial Y-TZP (T, ST, XT, and P), containing different amount of cubic crystal, were examined. Artificial aging was accomplished by autoclaving at 122°C under 2 bar pressure for 8 hours. Fatigue simulation parameters were set using an axial 50 N load, a total of 240,000 cycles. Flexural fatigue strength was evaluated.

STATISTICAL ANALYSIS

Two-way analysis of variance with Tukey's honestly significant difference test was used to determine the difference in fatigue strength values between various type of zirconia materials within control and aging with a significant level of 5%. Weibull analysis was conducted on the fatigue strength data.

RESULTS

All groups showed the mean flexural fatigue strength had no significant difference in hydrothermally aged specimens compared with specimens without aging ( = 0.154). Group T showed significantly higher flexural fatigue strength followed by group ST, XT, and P. Group XT and P showed no significant difference in strength value ( > 0.05). Group T demonstrated a lower probability of failure than group ST, XT, and P whether with or without aging. Weibull modulus in group T and ST with aging condition was increased and higher than all the experimental groups.

CONCLUSION

Cubic-containing zirconia materials (group ST, XT, and P) exhibited lower flexural fatigue strength than non-cubic 3Y-TZP zirconia (group T). However, various cubic-containing translucent zirconia was assumed to have high resistance to hydrothermal degradation.

摘要

目的

本研究旨在探究含立方相的半透明钇稳定四方氧化锆多晶体(Y-TZP)的疲劳及水热降解行为。

材料与方法

对四组含有不同立方相晶体含量的商用Y-TZP(T、ST、XT和P)进行检测。人工老化通过在122°C、2巴压力下高压灭菌8小时来完成。使用轴向50 N载荷、总共240,000次循环设置疲劳模拟参数。评估弯曲疲劳强度。

统计分析

采用双因素方差分析及Tukey真实显著性差异检验来确定在对照和老化条件下不同类型氧化锆材料之间疲劳强度值的差异,显著性水平为5%。对疲劳强度数据进行威布尔分析。

结果

所有组均显示,与未老化的试样相比,水热老化试样的平均弯曲疲劳强度无显著差异(P = 0.154)。T组的弯曲疲劳强度显著高于ST组、XT组和P组。XT组和P组在强度值上无显著差异(P > 0.05)。无论老化与否,T组的失效概率均低于ST组、XT组和P组。老化条件下T组和ST组的威布尔模量增加且高于所有实验组。

结论

含立方相的氧化锆材料(ST组、XT组和P组)的弯曲疲劳强度低于不含立方相的3Y-TZP氧化锆(T组)。然而,各种含立方相的半透明氧化锆被认为具有高水热降解抗性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f366/10569846/af3e567a90ea/10-1055-s-0042-1755630-i2252138-1.jpg

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