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一种新型Al-Zn-Mg-Li-Cu合金的热变形行为及微观组织演变

Hot Deformation Behavior and Microstructure Evolution of a Novel Al-Zn-Mg-Li-Cu Alloy.

作者信息

Wu Shuaishuai, Zhu Baohong, Jiang Wei, Qiu Haochen, Guo Yang

机构信息

GRIMAT Engineering Institute Co., Ltd., Beijing 101407, China.

General Research Institute for Nonferrous Metals, Beijing 100088, China.

出版信息

Materials (Basel). 2022 Sep 29;15(19):6769. doi: 10.3390/ma15196769.

Abstract

Lightweight structural alloys have broad application prospects in aerospace, energy, and transportation fields, and it is crucial to understand the hot deformation behavior of novel alloys for subsequent applications. The deformation behavior and microstructure evolution of a new Al-Zn-Mg-Li-Cu alloy was studied by hot compression experiments at temperatures ranging from 300 °C to 420 °C and strain rates ranging from 0.01 s to 10 s. The as-cast Al-Zn-Mg-Li-Cu alloy is composed of an α-Al phase, an AlCu phase, a T phase, an η phase, and an η' phase. The constitutive relationship between flow stress, temperature, and strain rate, represented by Zener-Hollomon parameters including Arrhenius terms, was established. Microstructure observations show that the grain size and the fraction of DRX increases with increasing deformation temperature. The grain size of DRX decreases with increasing strain rates, while the fraction of DRX first increases and then decreases. A certain amount of medium-angle grain boundaries (MAGBs) was present at both lower and higher deformation temperatures, suggesting the existence of continuous dynamic recrystallization (CDRX). The cumulative misorientation from intragranular to grain boundary proves that the CDRX mechanism of the alloy occurs through progressive subgrain rotation. This paper provides a basis for the deformation process of a new Al-Zn-Mg-Li-Cu alloy.

摘要

轻质结构合金在航空航天、能源和交通领域具有广阔的应用前景,了解新型合金的热变形行为对于后续应用至关重要。通过在300℃至420℃的温度范围和0.01s至10s的应变速率下进行热压缩实验,研究了一种新型Al-Zn-Mg-Li-Cu合金的变形行为和微观组织演变。铸态Al-Zn-Mg-Li-Cu合金由α-Al相、AlCu相、T相、η相和η'相组成。建立了以包含阿累尼乌斯项的齐纳-霍洛蒙参数表示的流动应力、温度和应变速率之间的本构关系。微观组织观察表明,动态再结晶(DRX)的晶粒尺寸和体积分数随变形温度的升高而增加。DRX的晶粒尺寸随应变速率的增加而减小,而DRX的体积分数先增加后减小。在较低和较高的变形温度下均存在一定数量的中角度晶界(MAGB),表明存在连续动态再结晶(CDRX)。从晶内到晶界的累积取向差证明了该合金的CDRX机制是通过渐进亚晶粒旋转发生的。本文为新型Al-Zn-Mg-Li-Cu合金的变形过程提供了依据。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a108/9573753/8edc58994dc4/materials-15-06769-g001.jpg

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