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基于双相镁锂基合金加工图的热变形行为及微观组织演变

Hot Deformation Behavior and Microstructural Evolution Based on the Processing Map of Dual-Phase Mg-Li Based Alloy.

作者信息

Guo Jiangtao, Guo Shengli, Shen Yazhao, Li Defu

机构信息

State Key Laboratory of Nonferrous Metals and Processes, GRINM Group Co., Ltd., Beijing 101407, China.

GRIMAT Engineering Institute Co., Ltd., Beijing 101407, China.

出版信息

Materials (Basel). 2022 Jan 28;15(3):1022. doi: 10.3390/ma15031022.

Abstract

The deformation behavior of the as-extruded Mg-Li-Al-Zn-Si alloy was studied by conducting a hot compression test, with a temperature range of 180-330 °C and a strain rate range of 0.01-10 s. The constitutive relationship of flow stress, temperature, and strain rate was expressed by the Zener-Hollomon parameter and included the Arrhenius term. By considering the effect of strain on the material constants, the flow stress at 240-330 °C could be precisely predicted with the constitutive equation (incorporating the influence of strain). A processing map was established at the strain of 0.7. The unsafe domains that are characterized by uneven microstructures were detected at low temperatures (<230 °C) or high temperatures (>280 °C), with high strain rates (>1 s). The optimum hot deformation region was obtained at a medium temperature (270-300 °C), with a peak power dissipation efficiency of 0.44. The microstructural evolution in different domains is investigated. The unstable domains are characterized by a non-uniform flow behavior and uneven microstructure. The observation showed that the dynamic recrystallization (DRX) process could easily occur at the safe domain with high power dissipation efficiency. For the α-phase, some features of continuous dynamic recrystallization can be found. The triple points serve as prominent nucleation sites for the β-phase DRX grains and the growth in the grains was carried out by subgrain boundary migration. The microstructure exhibits characteristics of discontinuous dynamic recrystallization.

摘要

通过进行热压缩试验研究了挤压态Mg-Li-Al-Zn-Si合金的变形行为,试验温度范围为180-330℃,应变速率范围为0.01-10s⁻¹。流动应力、温度和应变速率之间的本构关系由Zener-Hollomon参数表示,并包含Arrhenius项。考虑应变对材料常数的影响,利用本构方程(考虑应变的影响)可以精确预测240-330℃下的流动应力。在应变为0.7时建立了加工图。在低温(<230℃)或高温(>280℃)、高应变速率(>1s⁻¹)下检测到以微观结构不均匀为特征的不安全区域。在中等温度(270-300℃)下获得了最佳热变形区域,峰值功率耗散效率为0.44。研究了不同区域的微观组织演变。不稳定区域的特征是流动行为不均匀和微观结构不均匀。观察表明,在具有高功率耗散效率的安全区域容易发生动态再结晶(DRX)过程。对于α相,可以发现一些连续动态再结晶的特征。三相点是β相DRX晶粒的突出形核位置,晶粒生长通过亚晶界迁移进行。微观结构呈现出不连续动态再结晶的特征。

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