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分析不同部位的旋覆花中的挥发性化合物

Analysis of Volatile Compounds from Different Parts of Thunb.

机构信息

Taoyuan District Agricultural Research and Extension Station, Council of Agriculture, Executive Yuan, Taoyuan 327, Taiwan.

Department of Cosmeceutics, China Medical University, Taichung 406, Taiwan.

出版信息

Molecules. 2022 Dec 14;27(24):8893. doi: 10.3390/molecules27248893.

Abstract

Thunb. is a medicinal and edible plant that has been commonly used in traditional Chinese medicine since ancient times. This study used headspace solid-phase microextraction (HS-SPME) and direct injection, combined with gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS), to identify the volatile compounds in Extraction from different parts of the plant using different extraction techniques for the identification of volatile compounds were determined. A total of 93 volatile components were analyzed in the leaves, stems, rhizomes, and whole plant samples of . The leaves contained more ()-3-hexenal, β-myrcene, ()-β-ocimene, and (4,6)--ocimene; the stems contained more geranyl acetate and nerolidol; and rhizomes contained more α-pinene, β-pinene, limonene, 2-undecanone, and decanoyl acetaldehyde. Among them, the essential oil extracted by HS-SPME could produce more monoterpenes, while direct injection could obtain higher contents of aliphatic ketones, terpene esters, sesquiterpenes, and was more conducive to the extraction of 2-undecanone and decanoyl acetaldehyde.

摘要

竹柏是一种药食两用植物,自古以来就在中医药中被广泛应用。本研究采用顶空固相微萃取(HS-SPME)和直接进样,结合气相色谱(GC)和气相色谱-质谱联用(GC-MS),对植物不同部位的挥发油进行了鉴定。采用不同的提取技术,从竹叶、竹茎、竹根和全株中提取了竹柏的挥发油成分。共分析了竹叶、竹茎、竹根和全株样品中的 93 种挥发性成分。叶片中含有更多的()-3-己烯醛、β-月桂烯、()-β-罗勒烯和(4,6)-对伞花烃;茎中含有更多的乙酸香叶酯和橙花叔醇;而根中则含有更多的α-蒎烯、β-蒎烯、柠檬烯、2-十一酮和癸酰基乙醛。其中,HS-SPME 提取的精油可以产生更多的单萜,而直接进样则可以获得更高含量的脂肪族酮、萜烯酯、倍半萜烯,并且更有利于 2-十一酮和癸酰基乙醛的提取。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f42f/9783048/b72af580467c/molecules-27-08893-g001a.jpg

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