Taoyuan District Agricultural Research and Extension Station, Council of Agriculture, Executive Yuan, Taoyuan 327, Taiwan.
Department of Cosmeceutics, China Medical University, Taichung 406, Taiwan.
Molecules. 2022 Dec 14;27(24):8893. doi: 10.3390/molecules27248893.
Thunb. is a medicinal and edible plant that has been commonly used in traditional Chinese medicine since ancient times. This study used headspace solid-phase microextraction (HS-SPME) and direct injection, combined with gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS), to identify the volatile compounds in Extraction from different parts of the plant using different extraction techniques for the identification of volatile compounds were determined. A total of 93 volatile components were analyzed in the leaves, stems, rhizomes, and whole plant samples of . The leaves contained more ()-3-hexenal, β-myrcene, ()-β-ocimene, and (4,6)--ocimene; the stems contained more geranyl acetate and nerolidol; and rhizomes contained more α-pinene, β-pinene, limonene, 2-undecanone, and decanoyl acetaldehyde. Among them, the essential oil extracted by HS-SPME could produce more monoterpenes, while direct injection could obtain higher contents of aliphatic ketones, terpene esters, sesquiterpenes, and was more conducive to the extraction of 2-undecanone and decanoyl acetaldehyde.
竹柏是一种药食两用植物,自古以来就在中医药中被广泛应用。本研究采用顶空固相微萃取(HS-SPME)和直接进样,结合气相色谱(GC)和气相色谱-质谱联用(GC-MS),对植物不同部位的挥发油进行了鉴定。采用不同的提取技术,从竹叶、竹茎、竹根和全株中提取了竹柏的挥发油成分。共分析了竹叶、竹茎、竹根和全株样品中的 93 种挥发性成分。叶片中含有更多的()-3-己烯醛、β-月桂烯、()-β-罗勒烯和(4,6)-对伞花烃;茎中含有更多的乙酸香叶酯和橙花叔醇;而根中则含有更多的α-蒎烯、β-蒎烯、柠檬烯、2-十一酮和癸酰基乙醛。其中,HS-SPME 提取的精油可以产生更多的单萜,而直接进样则可以获得更高含量的脂肪族酮、萜烯酯、倍半萜烯,并且更有利于 2-十一酮和癸酰基乙醛的提取。