Wu Changlong, Chen Shuang, Tang Jie, Fu Dingfa, Teng Jie, Jiang Fulin
College of Materials Science and Engineering, Hunan University, Changsha 410082, China.
Hunan Provincial Key Laboratory of Vehicle Power and Transmission System, Hunan Institute of Engineering, Xiangtan 411104, China.
Materials (Basel). 2023 Jan 13;16(2):796. doi: 10.3390/ma16020796.
The size and distribution of ceramic particles in aluminum matrix composites have been reported to remarkably influence their properties. For a single ceramic particle, the particle size is too small and prone to agglomeration, which makes the mechanical properties of the composites worse. When the ceramic particle size is too large, the particles and alloy at the interface are not firmly bonded, and the effect of dispersion distribution is not achieved, which will also reduce the mechanical properties of the composites. The multi-size ceramic particles are expected to improve this situation, while their effect on hot workability is less studied. In this study, the hot deformation behavior, constitutive model, processing map and SEM microstructure were investigated to evaluate the hot workability of multi-size SiC particle-reinforced 6013 aluminum matrix composites. The results showed that the increased deformation temperature and decreased strain rate could decrease flow stresses. The flow stress behaviors of the composites can be described by the sine-hyperbolic Arrhenius equation with the deformation activation energy of Q = 205.863 kJ/mol. The constitutive equation of the composites is ε ˙=3.11592×1013sinh0.024909σ4.12413exp−205863RT. Then, the hot processing map of the SiCp/6013 composites was constructed and verified by SEM observations. The rheological instability zone was in the region of a high strain rate. The optimal processing zone for composites was 450500 °C and 0.030.25 s−1. In addition, the strain level was found to increase both the Q value and the area of the instability zone.
据报道,铝基复合材料中陶瓷颗粒的尺寸和分布对其性能有显著影响。对于单个陶瓷颗粒,颗粒尺寸过小且容易团聚,这会使复合材料的力学性能变差。当陶瓷颗粒尺寸过大时,颗粒与界面处的合金结合不牢固,无法实现弥散分布效果,这也会降低复合材料的力学性能。多尺寸陶瓷颗粒有望改善这种情况,但其对热加工性能的影响研究较少。在本研究中,通过研究热变形行为、本构模型、加工图和扫描电镜微观结构来评估多尺寸SiC颗粒增强6013铝基复合材料的热加工性能。结果表明,变形温度升高和应变速率降低会降低流变应力。复合材料的流变应力行为可用正弦双曲阿累尼乌斯方程描述,其变形激活能Q = 205.863 kJ/mol。复合材料的本构方程为ε˙=3.11592×1013sinh0.024909σ4.12413exp−205863RT。然后,构建了SiCp/6013复合材料的热加工图,并通过扫描电镜观察进行了验证。流变失稳区位于高应变速率区域。复合材料的最佳加工区为450500 °C和0.030.25 s−1。此外,发现应变水平会增加Q值和失稳区面积。