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巴西身体油中甜杏仁油的气相色谱和质谱质量和纯度评估的首次报告。

First report on quality and purity assessment of sweet almond oil in Brazilian body oils by gas chromatography and mass spectrometry.

机构信息

Department of Chemistry, State University of Maringá (UEM), Maringá, Paraná, 87020-900, Brazil.

Post-Graduate Program in Food Science, State University of Maringá (UEM), Maringá, Paraná, 87020-900, Brazil.

出版信息

J Mass Spectrom. 2023 Jan;58(1):e4900. doi: 10.1002/jms.4900.

Abstract

Sweet almond oil is a raw material with high-added value used in different products. Then, the aim of this study is to evaluate the quality and purity of 10 body oils based on sweet almond oils currently available in the Brazilian market. Fatty acid composition and triacylglycerol (TAG) profile were determined by gas chromatography with flame ionization detector (GC-FID) and atmospheric solids analysis probe mass spectrometry (ASAP-MS), respectively. The authenticity of samples was assessed using an analytical curve equation. Soybean oil was chosen as the adulterant because it is the cheapest vegetable oil commercialized in Brazil. Hierarchical clustering analysis (HCA) in conjunction with ASAP-MS classified product samples according to the type of vegetable oil (soybean and sweet almond oils). The addition of soybean oil (8.79% to 99.70%) was confirmed in samples. However, only two samples stated in their label the presence of soybean oil as an ingredient. These findings highlight the need for better oversight by regulatory bodies to ensure that consumers acquire high quality and authentic products based on equally high quality and purity of sweet almond oils.

摘要

甜杏仁油是一种高附加值的原料,用于不同的产品。因此,本研究旨在评估目前巴西市场上 10 种杏仁油基础身体油的质量和纯度。脂肪酸组成和三酰基甘油(TAG)谱分别通过气相色谱法(GC-FID)和大气压固体分析探针质谱法(ASAP-MS)进行测定。使用分析曲线方程评估样品的真实性。选择大豆油作为掺杂物,因为它是巴西市场上最便宜的植物油。结合 ASAP-MS 的层次聚类分析(HCA)根据植物油的类型(大豆油和甜杏仁油)对产品样品进行分类。在样品中确认添加了大豆油(8.79%至 99.70%)。然而,只有两个样品在标签上注明含有大豆油作为一种成分。这些发现强调了监管机构需要更好地监督,以确保消费者获得高质量和纯正的产品,这些产品基于同样高质量和高纯度的甜杏仁油。

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