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带有高数值孔径的用于二次离子质谱法的 Schwarzschild 显微镜的设计方法和结构。

Design method and construction of the Schwarzschild microscope with high numerical aperture for secondary ion mass spectrometry.

机构信息

CAS Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, Liaoning 116023, People's Republic of China.

College of Instrumentation and Electrical Engineering, Jilin University, 938 Ximinzhu Road, Changchun, Jilin 130061, People's Republic of China.

出版信息

Rev Sci Instrum. 2023 Jan 1;94(1):013701. doi: 10.1063/5.0128170.

Abstract

The Schwarzschild microscope is suitable for sample navigation in secondary ion mass spectrometry (SIMS) because of its advantages of a simple structure, large working distance, and good coordination with the ion extraction system. The high numerical aperture (NA) of the microscope significantly reduces diffraction effects, but the resulting high-order geometric aberrations seriously affect the imaging quality. In this paper, a novel design method of the Schwarzschild microscope with a high NA (0.47) was proposed. The aberration distributions and compensation methods were investigated through tolerance analysis. The results showed that the tilt and decenter tolerances become the dominant factors limiting the spatial resolution, which could only be improved by ensuring the alignment accuracy of mirrors. Finally, the spatial resolution of the microscope in the home-built SIMS reached 2.19 µm.

摘要

施瓦西显微镜因其结构简单、工作距离大、与离子引出系统协调性好等优点,适用于二次离子质谱(SIMS)中的样品导航。显微镜的高数值孔径(NA)显著降低了衍射效应,但由此产生的高阶几何像差严重影响了成像质量。本文提出了一种具有高数值孔径(0.47)的施瓦西显微镜的新型设计方法。通过公差分析研究了像差分布和补偿方法。结果表明,倾斜和偏心公差成为限制空间分辨率的主要因素,只能通过确保镜子的对准精度来提高。最后,自行研制的 SIMS 中的显微镜空间分辨率达到 2.19 µm。

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