Kim F H, Yeung H, Garboczi E J
National Institute of Standards and Technology, Intelligent Systems Division, Gaithersburg, MD, USA.
National Institute of Standards and Technology, Applied Chemicals and Materials Division, Boulder, CO, USA.
Addit Manuf. 2021 Dec;48(A). doi: 10.1016/j.addma.2021.102372.
Near-surface or sub-surface pores are critical to the structural integrity of additively manufactured (AM) metal parts, especially in fatigue failure applications. However, their formation in laser powder bed fusion is not well-understood due to the complex processes happening near the surface, which are challenging to monitor. A lack of high-fidelity data hinders understanding of the process and its effects. It is not well-known that problems with laser control parameters such as galvanometer acceleration and laser power on/off delay can form near-surface pores in laser powder bed fusion (LPBF) AM processes, and we investigated the characteristics of these pores in this research. We also demonstrate the capabilities and processes of combined studies using in-situ melt pool images and ex-situ X-ray computed tomography (XCT) images. Using the National Institute of Standards and Technology (NIST) Additive Manufacturing Metrology Testbed (AMMT), varying laser control schemes were implemented while in-situ coaxial melt pool images were acquired during the build of Nickel superalloy parts. A combination of time-stepped digital commands, in-situ coaxial melt pool monitoring images (≈ 8 μm/pixel), and ex-situ high-resolution XCT images (≈ 3.63 μm/voxel) were demonstrated. Advanced image analysis methods were used to characterize the pores found in terms of size and shape distribution and spatial location. XCT images, in high correspondence to melt pool images, clearly show the effects of the laser control parameters. We present the complete analysis chain of AM command, in-situ melt pool imaging, ex-situ XCT acquisition, and image analysis. Possible near-surface pore formation mechanisms are explained through the comparative image analysis. The approach of compiling combined analyses based on time-stepped digital commands, in-situ monitoring results, and ex-situ XCT measurement through image analysis enables observation and categorization of the different near-surface pore formation mechanisms stemming from laser and scan control.
近表面或亚表面孔隙对于增材制造(AM)金属零件的结构完整性至关重要,尤其是在疲劳失效应用中。然而,由于表面附近发生的复杂过程难以监测,它们在激光粉末床熔融过程中的形成机制尚未得到很好的理解。缺乏高保真数据阻碍了对该过程及其影响的理解。尚不清楚诸如振镜加速度和激光功率开/关延迟等激光控制参数问题会在激光粉末床熔融(LPBF)增材制造过程中形成近表面孔隙,我们在本研究中对这些孔隙的特性进行了研究。我们还展示了使用原位熔池图像和非原位X射线计算机断层扫描(XCT)图像进行联合研究的能力和过程。利用美国国家标准与技术研究院(NIST)的增材制造计量试验台(AMMT),在制造镍基高温合金零件的过程中,实施了不同的激光控制方案,同时采集了原位同轴熔池图像。展示了时间步长数字命令、原位同轴熔池监测图像(≈8μm/像素)和非原位高分辨率XCT图像(≈3.63μm/体素)的组合。采用先进的图像分析方法,从尺寸、形状分布和空间位置方面对发现的孔隙进行表征。与熔池图像高度对应的XCT图像清楚地显示了激光控制参数的影响。我们展示了增材制造命令、原位熔池成像、非原位XCT采集和图像分析的完整分析链。通过对比图像分析解释了可能的近表面孔隙形成机制。基于时间步长数字命令、原位监测结果和通过图像分析的非原位XCT测量来编制联合分析的方法,能够观察和分类源于激光和扫描控制的不同近表面孔隙形成机制。