Pimentel Eliene Soares, França Fabiana Mantovani Gomes, Turssi Cecilia Pedroso, Basting Roberta Tarkany, Vieira-Junior Waldemir Francisco
Faculdade São Leopoldo Mandic, Instituto de Pesquisas São Leopoldo Mandic, Rua José Rocha Junqueira, 13, Campinas, SP, CEP, 13045-755, Brazil.
Clin Oral Investig. 2023 Jul;27(7):3545-3556. doi: 10.1007/s00784-023-04968-6. Epub 2023 Mar 30.
To evaluate the effect of acid erosion on different physical properties of resin composite with S-PRG (surface pre-reacted glass) fillers, by conducting simulations of intrinsic and extrinsic sources.
Cylindrical samples (Ø6 vs. 2 mm) of a conventional nanohybrid resin composite (Forma, Ultradent) and of a nanohybrid resin composite with S-PRG filler (Beautifil II, Shofu) were exposed to erosive cycling (5 days), based on (n=12) remineralizing solution (control); 0.3% citric acid (pH=2.6); or 0.01 M hydrochloric acid (pH=2). Roughness (Ra), microhardness (KHN), and color (CIELab*, CIEDE2000, and Vita scale (SGU)) factors were analyzed at the initial and final time points, and the general color changes (ΔE, ΔE, ΔSGU) were calculated. Final images were obtained using scanning electron microscopy (SEM). The data were evaluated by generalized models, Mann-Whitney, Wilcoxon, Kruskal-Wallis, and Dunn tests (α=0.05).
Regarding KHN, there was no difference between the groups or the time periods (p = 0.74). As for Ra, there was a significant increase in the Ra of both composites after cycling with hydrochloric acid, but only the resin composite with S-PRG filler showed a change in Ra after cycling with citric acid (p = 0.003). After cycling with citric and hydrochloric acid, the highest Ra values were found for the resin composite with S-PRG filler (p < 0.0001), corroborating the result of images (SEM) indicating loss of filler and porosities in this material. The resin composite with S-PRG filler showed higher ΔE and ΔE, in addition to more negative ΔSGU values and lower L* values after exposure to both acids, compared to the control (p < 0.05).
The acidic conditions altered the roughness and color stability of the materials tested, pointing out that the resin composite containing S-PRG filler showed greater degradation of its physical properties than the conventional resin composite.
Bioactive materials are relevant, considering that their properties interact with dental hard tissues; however, the S-PRG-based resin composite showed greater degradation under acidic conditions than the conventional resin composite.
通过对内在和外在酸蚀源进行模拟,评估酸蚀对含S-PRG(表面预反应玻璃)填料的树脂复合材料不同物理性能的影响。
将常规纳米混合树脂复合材料(Forma,Ultradent)和含S-PRG填料的纳米混合树脂复合材料(Beautifil II,Shofu)的圆柱形样本(直径6对2毫米)置于侵蚀循环(5天)环境中,基于(n = 12)再矿化溶液(对照);0.3%柠檬酸(pH = 2.6);或0.01 M盐酸(pH = 2)。在初始和最终时间点分析粗糙度(Ra)、显微硬度(KHN)和颜色(CIELab*、CIEDE2000和Vita比色板(SGU))因素,并计算总体颜色变化(ΔE、ΔE、ΔSGU)。使用扫描电子显微镜(SEM)获取最终图像。通过广义模型、Mann-Whitney检验、Wilcoxon检验、Kruskal-Wallis检验和Dunn检验(α = 0.05)对数据进行评估(α = 0.05)。
关于KHN,各组之间以及各时间段之间均无差异(p = 0.74)。至于Ra,两种复合材料在盐酸侵蚀循环后Ra均显著增加,但只有含S-PRG填料的树脂复合材料在柠檬酸侵蚀循环后Ra发生了变化(p = 0.003)。在柠檬酸和盐酸侵蚀循环后,含S-PRG填料的树脂复合材料的Ra值最高(p < 0.0001),这与图像(SEM)结果一致,表明该材料中填料流失且出现孔隙。与对照组相比,含S-PRG填料的树脂复合材料在暴露于两种酸后显示出更高的ΔE和ΔE,此外ΔSGU值更负且L*值更低(p < 0.05)。
酸性条件改变了所测试材料的粗糙度和颜色稳定性,表明含S-PRG填料的树脂复合材料比传统树脂复合材料的物理性能降解更严重。
考虑到生物活性材料的性能与牙体硬组织相互作用,生物活性材料具有相关性;然而,基于S-PRG的树脂复合材料在酸性条件下比传统树脂复合材料表现出更大程度的降解。