Department of Restorative Dentistry, School of Dentistry, University of Bolu Abant Izzet Baysal, Bolu, Turkey.
Department of Restorative Dentistry, School of Dentistry, University of Istanbul Medeniyet, Orhanlı-Tuzla Campus, Istanbul, 34956, Turkey.
Odontology. 2024 Oct;112(4):1197-1208. doi: 10.1007/s10266-024-00932-2. Epub 2024 Apr 3.
The aim of this study is to investigate the repair bond strength of composite resin following three different surface treatments (bur-grinding, silanization, and Er,Cr:YSGG laser irradiation) using various universal adhesives. A total of 160 resin composite specimens, produced in cylindrical form (6 × 2 mm) with a nanohybrid composite resin within metal molds, were subjected to 5000 cycles of aging in a thermocycler. The aged samples were categorized into four groups based on surface treatments: control, bur, silane, and Er,Cr:YSGG laser. Following surface treatments, the specimens underwent repair using the same resin composite and four different adhesive systems: Tokuyama Universal Bond (TUB), Prime Bond Universal (PBU), Gluma Bond Universal (GBU), and Clearfil SE Bond (CSB). Subsequently, the specimens were subjected to shear forces, and statistical analysis was performed using two-way ANOVA and Tukey tests (p < 0.05). The failure modes were examined using a stereomicroscope, and the surface topography of the roughened resin composite was assessed through scanning electron microscopy (SEM). Results indicated that silane + GBU exhibited the highest shear bond strength (SBS) (15.61 MPa) while control + TUB showed the lowest SBS (7.63 MPa). Silane demonstrated significantly higher SBS values (p ≤ 0.05), with no significant difference observed between bur and laser methods (p = 0.998). It is recommended to include an additional silanization step before applying universal adhesive, as it effectively enhances the bond strength of the repaired composite.
本研究旨在探讨三种不同表面处理(打磨、硅烷化和 Er,Cr:YSGG 激光处理)条件下,使用不同通用粘结剂对复合树脂的修复粘结强度。共制备 160 个圆柱形复合树脂试件(6×2mm),将纳米复合树脂置于金属模具内,在热循环仪中进行 5000 次老化循环。将老化后的样本根据表面处理方法分为四组:对照组、打磨组、硅烷组和 Er,Cr:YSGG 激光组。进行表面处理后,使用相同的复合树脂和四种不同的粘结系统(Tokuyama Universal Bond [TUB]、Prime Bond Universal [PBU]、Gluma Bond Universal [GBU]和 Clearfil SE Bond [CSB])对试件进行修复。随后,对试件进行剪切力测试,并使用双向方差分析和 Tukey 检验(p<0.05)进行统计分析。使用体视显微镜检查失效模式,并通过扫描电子显微镜(SEM)评估粗糙化复合树脂的表面形貌。结果表明,硅烷+GBU 表现出最高的剪切粘结强度(SBS)(15.61 MPa),而对照组+TUB 表现出最低的 SBS(7.63 MPa)。硅烷处理显示出显著更高的 SBS 值(p≤0.05),但打磨和激光方法之间没有显著差异(p=0.998)。建议在使用通用粘结剂之前增加额外的硅烷化步骤,因为它可以有效提高修复复合树脂的粘结强度。