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Synthesis and crystal structure of -(5-acetyl-4-methyl-pyrimidin-2-yl)benzene-sulfonamide.

作者信息

Mohamed-Ezzat Reham A, Kariuki Benson M, Azzam Rasha A

机构信息

Chemistry of Natural & Microbial Products Department, National Research Center, Cairo, Egypt.

School of Chemistry, Cardiff University, Main Building, Park Place, Cardiff CF10, 3AT, United Kingdom.

出版信息

Acta Crystallogr E Crystallogr Commun. 2023 Mar 15;79(Pt 4):331-334. doi: 10.1107/S2056989023001871. eCollection 2023 Mar 1.

Abstract

-(5-Acetyl-4-methyl-pyrimidin-2-yl)benzene-sulfonamide, CHNOS, was sythesized and characterized by single-crystal X-ray diffraction. In the crystal, π-π inter-actions between the phenyl and pyrimidine groups of neighbouring mol-ecules form mol-ecular chains parallel to [010]. Adjacent mol-ecular chains are linked by N-H⋯N hydrogen-bonding inter-actions between the pyrimidine and amine groups of neighbouring mol-ecules, resulting in a three-dimensional network.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/57e7/10088322/590d394b0010/e-79-00331-fig1.jpg

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