Sheeba Kasirajan Rajam Jaya, Priya Retnam Krishna, Arunachalam Krishna Prakash, Avudaiappan Siva, Maureira-Carsalade Nelson, Roco-Videla Ángel
PG & Research Department of Physics, Holy Cross College (Autonomous), Manonmaniam Sundaranar University, Nagercoil 627012, Tamil Nadu, India.
Department of Civil Engineering, College of Engineering Nagercoil, Anna University, Kanyakumari 629004, India.
Polymers (Basel). 2023 Apr 23;15(9):1996. doi: 10.3390/polym15091996.
The present study concerns the physico-chemical, structural, mechanical and thermal characterization of Acacia pennata, a natural and almost inexpensive fibre, as a potential reinforcement in polymer composites. The effect of treating the fibre with sodium acetate to increase its qualities has been seen through the use of thermogravimetric analysis, scanning electron microscope (SEM) analysis, X-ray diffraction (XRD), mechanical property tester, and Fourier transform infrared spectroscopy (FTIR). According to XRD analysis, the elimination of lignin and wax-like impurities resulted in an increase in the AP fibre's crystalline index (79.73%). The fibre's thermal stability was also discovered to be 365 °C. Tensile strength (557.58 MPa) and elongation at break both increased by 2.9% after treatment with sodium acetate. The surface nature and quality of AP fibres improved after sodium acetate treatment. It was confirmed by the reduction of chemical compositions (such as hemicellulose, lignin and pectin). Given its density, the fibre can be suggested as a reinforcement in polymer composites for light-weight applications because its lightweight property will be more useful for composite manufacturing.
本研究关注的是作为聚合物复合材料潜在增强材料的藤金合欢这种天然且几乎廉价的纤维的物理化学、结构、机械和热性能表征。通过热重分析、扫描电子显微镜(SEM)分析、X射线衍射(XRD)、机械性能测试仪和傅里叶变换红外光谱(FTIR),观察到用醋酸钠处理纤维以提高其性能的效果。根据XRD分析,木质素和蜡状杂质的去除导致藤金合欢纤维的结晶指数增加(79.73%)。还发现该纤维的热稳定性为365℃。用醋酸钠处理后,拉伸强度(557.58MPa)和断裂伸长率均提高了2.9%。醋酸钠处理后,藤金合欢纤维的表面性质和质量得到改善。化学成分(如半纤维素、木质素和果胶)的减少证实了这一点。鉴于其密度,该纤维可被建议用作聚合物复合材料中用于轻质应用的增强材料,因为其轻质特性对复合材料制造将更有用。