Federal State Budgetary Institution "Technological Institute for Superhard and Novel Carbon Materials" (FSBI TISNCM), Troitsk, 108840 Moscow, Russia.
Sensors (Basel). 2023 May 5;23(9):4502. doi: 10.3390/s23094502.
The application of microwave diamond-based HBAR as a sensor of microwave acoustic attenuation α was considered, using the Mo film as an object of research. A multilayered piezoelectric structure, as the Al/AlScN/Mo/(100) diamond/Mo, was produced using aluminum-scandium nitride composition, and was studied in detail for a number of the Mo films with different thicknesses obtained by magnetron deposition. The operational frequency band of 3.3 … 18 GHz was used. It was found that the dependence of the resonant frequency shift vs. the (Mo) thickness for all the overtones to be investigated was linear. For a given sensor, it was found that the mass sensitivity per unit area was equal to -26 × 10 and -8.7 × 10 g/(cm∙Hz) at 6.0 GHz and 18.3 GHz, respectively. The frequency dependencies of quality factor , which changed as a result of Mo film deposition, were considered as the basic experimental data. A method for extracting the α(Mo) values was proposed. The -factor under the complete deposition of Mo film was 936 nm, and dropped moderately to ~25%. Such values were enough for an aim of the given experiment. The α() in molybdenum was obtained, and demonstrated a dependence that was close to quadratic, corresponding to the Akhiezer attenuation law.
研究了将微波金刚石基 HBAR 应用于微波声衰减 α 的传感器,使用 Mo 膜作为研究对象。使用铝-钪氮化物组合制作了多层压电结构,即 Al/AlScN/Mo/(100) 金刚石/Mo,并详细研究了通过磁控溅射沉积获得的不同厚度的多个 Mo 膜。使用的工作频带为 3.3 … 18 GHz。结果发现,对于所有研究的泛音,共振频率偏移与 (Mo) 厚度的关系是线性的。对于给定的传感器,在 6.0 GHz 和 18.3 GHz 下,单位面积的质量灵敏度分别为 -26×10 和 -8.7×10 g/(cm∙Hz)。由于 Mo 膜沉积而变化的品质因数 Q 的频率依赖性被认为是基本的实验数据。提出了一种提取 α(Mo) 值的方法。Mo 膜完全沉积时的 - 因子为 936nm,并适度下降至~25%。这些值足以满足给定实验的目的。获得了 Mo 中的 α() 值,并证明了与 Akhiezer 衰减定律相对应的接近二次方的依赖关系。