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对来自(贾蒂贝)甘蔗的新型天然纤维素纤维作为聚合物复合材料潜在增强材料的表征。

Characterization of new natural cellulosic fiber from (Jati Bet) cane as a potential reinforcement for polymer composites.

作者信息

Kar Arup, Saikia Dip

机构信息

Department of Physics, Dibrugarh University, Assam, India.

Department of Physics, Digboi College, Digboi, Assam, India.

出版信息

Heliyon. 2023 May 23;9(6):e16491. doi: 10.1016/j.heliyon.2023.e16491. eCollection 2023 Jun.

Abstract

This study investigates the physical, structural, chemical, thermal, mechanical, and morphological properties of the fibers of canes and compares the findings with various lignocellulosic fibers to find the place of these fibers as reinforcements for polymer composites. Chemical analysis confirms the presence of 37.43 ± 1.40% cellulose, 31.06 ± 1.03% hemicellulose, and 28.42 ± 0.81% lignin in cane fibers, moreover, the presence of these constituents is also confirmed by Fourier Transformed Infrared Spectroscopic (FTIR) analysis. The X-Ray diffraction (XRD) analysis determines the crystallinity index of 37.38 ± 0.27% and the crystallite size of 0.87 ± 0.03 nm of the samples. The thermogravimetric analysis ensures that the cane fibers are thermally stable up to 210 ± 5 °C. The Weibull distribution analysis is employed to estimate the tensile properties of canes, which reveal a tensile strength of 37.5 ± 2 MPa, Young's modulus of 1.05 ± 0.08 GPa, and an elongation at break of 18.94 ± 4.26%. The roughness of the fibers' outer surface is confirmed by SEM micrographs and AFM analysis, suggesting that it could enhance the adhesion between fibers and matrix during the fabrication of composites.

摘要

本研究调查了藤茎纤维的物理、结构、化学、热学、力学和形态学特性,并将研究结果与各种木质纤维素纤维进行比较,以确定这些纤维作为聚合物复合材料增强材料的地位。化学分析证实藤茎纤维中含有37.43±1.40%的纤维素、31.06±1.03%的半纤维素和28.42±0.81%的木质素,此外,傅里叶变换红外光谱(FTIR)分析也证实了这些成分的存在。X射线衍射(XRD)分析确定了样品的结晶度指数为37.38±0.27%,微晶尺寸为0.87±0.03nm。热重分析表明藤茎纤维在210±5°C以下具有热稳定性。采用威布尔分布分析来估计藤茎的拉伸性能,结果显示其拉伸强度为37.5±2MPa,杨氏模量为1.05±0.08GPa,断裂伸长率为18.94±4.26%。扫描电子显微镜(SEM)照片和原子力显微镜(AFM)分析证实了纤维外表面的粗糙度,表明这可能会增强复合材料制造过程中纤维与基体之间的附着力。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bd7d/10238902/70f5f7c60c44/ga1.jpg

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