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具有“多色”颜色转变的当代CAD/CAM材料的物理化学性能评估

Evaluation of Physical-Chemical Properties of Contemporary CAD/CAM Materials with Chromatic Transition "Multicolor".

作者信息

Lukomska-Szymanska Monika, Radwanski Mateusz, Kharouf Naji, Mancino Davide, Tassery Herve, Caporossi Corrado, Inchingolo Francesco, de Almeida Neves Aline, Chou Yu Fu, Sauro Salvatore

机构信息

Department of General Dentistry, Medical University of Lodz, 251 Pomorska Str., 92-213 Lodz, Poland.

Department of Endodontics, Medical University of Lodz, 251 Pomorska Str., 92-213 Lodz, Poland.

出版信息

Materials (Basel). 2023 Jun 5;16(11):4189. doi: 10.3390/ma16114189.

Abstract

The use of materials for computer-aided design/computer-aided manufacturing (CAD/CAM) has been rapidly increasing in daily practice. However, one of the main issues regarding modern CAD/CAM materials is their aging in the oral environment, which may lead to significant changes in their overall properties. The aim of this study was to compare the flexural strength, water sorption, cross-link density (softening ratio%), surface roughness, and SEM analysis of three modern CAD/CAM "multicolor" composites. Grandio (Grandio disc multicolor-VOCO GmbH, Cuxhaven, Germany), Shofu (Shofu Block HC-Shofu Inc., Kyoto, Japan), and Vita (Vita Enamic multiColor-Vita Zahnfabrik, Bad Sackingen, Germany) were tested in this study. They were prepared in stick-shaped specimens and submitted to different tests after several aging protocols, such as thermocycling and mechanical cycle loading challenge. Further disc-shaped specimens were also created and tested for water sorption, cross-link density, surface roughness, and SEM ultramorphology, before and after storage in an ethanol-based solution. For flexural strength and ultimate tensile strength, Grandio showed the greatest values both at baseline and after aging ( < 0.05). Grandio and Vita Enamic presented the highest modulus of elasticity and the lowest water sorption ( < 0.05). A significant reduction ( < 0.05) in microhardness after ethanol storage (softening ratio%) was observed especially in Shofu. Grandio had the lowest roughness parameters compared to the other tested CAD/CAM materials, while ethanol storage significantly increased the Ra and RSm values in Shofu ( < 0.05). Despite the comparable modulus of elasticity of Vita and Grandio, this latter showed greater flexural strength and ultimate tensile strength both at baseline and after aging. Hence, Grandio and Vita Enamic may be employed for the anterior teeth and for those restorations requiring load-bearing capacity. Conversely, aging seems to affect several properties of Shofu, so its use for permanent restorations should be well-pondered based on the clinical situation.

摘要

计算机辅助设计/计算机辅助制造(CAD/CAM)材料在日常实践中的使用一直在迅速增加。然而,现代CAD/CAM材料的一个主要问题是它们在口腔环境中的老化,这可能导致其整体性能发生显著变化。本研究的目的是比较三种现代CAD/CAM“多色”复合材料的弯曲强度、吸水率、交联密度(软化率%)、表面粗糙度和扫描电子显微镜分析。本研究测试了Grandio(Grandio disc multicolor-VOCO GmbH,德国库克斯港)、松风(Shofu Block HC-松风株式会社,日本京都)和维他(Vita Enamic multiColor-维他齿科有限公司,德国巴特萨克京根)。将它们制备成棒状试样,并在经过几种老化方案(如热循环和机械循环加载挑战)后进行不同的测试。还制备了进一步的圆盘状试样,并在乙醇基溶液中储存前后测试其吸水率、交联密度、表面粗糙度和扫描电子显微镜超微结构。对于弯曲强度和极限拉伸强度,Grandio在基线和老化后均显示出最高值(P<0.05)。Grandio和Vita Enamic具有最高的弹性模量和最低的吸水率(P<0.05)。特别是在松风材料中,观察到乙醇储存后显微硬度显著降低(软化率%)(P<0.05)。与其他测试的CAD/CAM材料相比,Grandio的粗糙度参数最低,而乙醇储存显著增加了松风材料的Ra和RSm值(P<0.05)。尽管维他和Grandio的弹性模量相当,但后者在基线和老化后均显示出更大的弯曲强度和极限拉伸强度。因此,Grandio和Vita Enamic可用于前牙以及那些需要承载能力的修复体。相反,老化似乎会影响松风材料的几种性能,因此应根据临床情况慎重考虑将其用于永久性修复体。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3e3a/10254467/403d012f0e5d/materials-16-04189-g001.jpg

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