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现代修复性“生物活性”牙科材料的力学性能——一项体外研究。

Mechanical properties of modern restorative "bioactive" dental materials - an in vitro study.

作者信息

Radwanski Mateusz, Zmyslowska-Polakowska Ewa, Osica Karolina, Krasowski Michal, Sauro Salvatore, Hardan Louis, Lukomska-Szymanska Monika

机构信息

Department of Endodontics, Medical University of Lodz, Lodz, Poland.

Department of General Dentistry, Medical University of Lodz, 251 Pomorska Str, Lodz, 92-213, Poland.

出版信息

Sci Rep. 2025 Jan 28;15(1):3552. doi: 10.1038/s41598-025-86595-7.

Abstract

This study aimed at assessing the mechanical properties and degradation of commercial bioactive materials. The bioactive materials (Activa Bioactive Restorative, Beautifil Flow Plus F00, F03, Predicta Bulk Bioactive) and composite resin Filtek Supreme Flow were submitted to flexural and diametral tensile strength tests (FS, DTS), modulus of elasticity (ME) evaluation, and analysis of aging in 70% ethanol and saliva on their hardness and sorption. The results for DTS ranged from 33.16 MPa (Beautifil Flow Plus F03) to 47.74 MPa (Filtek Supreme Flow). The highest FS was 120.40 MPa (Predicta Bulk Bioactive), while the lowest values were 86.55 MPa (Activa Bioactive Restorative). Activa Bioactive Restorative showed the lowest ME, as well as the highest water sorption both in alcohol and artificial saliva. Moreover, aging in saliva induced a significant decrease in hardness for Activa Restorative (p < .01). Alcohol storage caused a significant decrease in hardness for all materials (p < .0001). All tested materials met the basic requirements for light-curing materials in terms of DTS and FS. However, all materials showed higher sorption in alcohol than in saliva, while hardness decreased significantly after 30 days. Predicta Bulk Bioactive presented the highest mechanical parameters, initial hardness, and the lowest sorption of alcohol and saliva.

摘要

本研究旨在评估市售生物活性材料的力学性能和降解情况。将生物活性材料(Activa生物活性修复材料、Beautifil Flow Plus F00、F03、Predicta块状生物活性材料)和复合树脂Filtek Supreme Flow进行弯曲和径向拉伸强度测试(FS、DTS)、弹性模量(ME)评估,并分析其在70%乙醇和唾液中老化后的硬度和吸附情况。DTS结果范围为33.16兆帕(Beautifil Flow Plus F03)至47.74兆帕(Filtek Supreme Flow)。最高的FS为120.40兆帕(Predicta块状生物活性材料),而最低值为86.55兆帕(Activa生物活性修复材料)。Activa生物活性修复材料的ME最低,在酒精和人工唾液中的吸水率也最高。此外,在唾液中老化导致Activa修复材料的硬度显著降低(p<0.01)。酒精储存导致所有材料的硬度显著降低(p<0.0001)。就DTS和FS而言,所有测试材料均满足光固化材料的基本要求。然而,所有材料在酒精中的吸附率均高于在唾液中的吸附率,且30天后硬度显著降低。Predicta块状生物活性材料具有最高的力学参数、初始硬度,以及最低的酒精和唾液吸附率。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9414/11775110/8dfc37639d2d/41598_2025_86595_Fig1_HTML.jpg

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