Chen Youming, Ud-Din Rafi, Yang Teng, Li Tao, Li Chuanghao, Chu Aimin, Zhao Yuping
Hunan Provincial Key Defense Laboratory of High Temperature Wear-Resisting Materials and Preparation Technology, School of Materials Science and Engineering, Hunan University of Science and Technology, Xiangtan 411201, China.
Materials Division, PINSTECH, Post Office Nilore, Islamabad 44000, Pakistan.
Materials (Basel). 2023 Jul 4;16(13):4819. doi: 10.3390/ma16134819.
AlO/Cu composite material (ACCM) are highly suitable for various advanced applications owing to its excellent properties. In the present work, a combination of the solution combustion synthesis and hydrogen reduction method was first employed to prepare AlO/Cu composite powder (ACCP), and subsequently ACCM was prepared by employing spark plasma sintering (SPS) technique. The effect of AlO contents and SPS temperatures on the properties (relative density, hardness, friction coefficient, and electrical conductivity, et al.) of ACCM were investigated in detail. The results indicated that ACCM was very dense, and microstructure was consisted of fine AlO particles evenly distributed in the Cu matrix. With the increase of SPS temperature, the relative density and hardness of ACCM had first increased and then decreased. At 775 °C, the relative density and hardness had attained the maximum values of 98.19% and 121.4 HV, respectively. With the increase of AlO content, although the relative density of ACCM had gradually decreased, nevertheless, its friction coefficient had increased. Moreover, with the increase of AlO contents, the hardness of ACCM first increased and then decreased, and reached the maximum value (121.4 HV) with 3 wt.% addition. On the contrary, the wear rate of ACCM had first decreased and then increased with the increase of AlO contents, and attained the minimum (2.32 × 10 mm/(N.m)) with 3 wt.% addition.
AlO/Cu复合材料(ACCM)因其优异的性能而非常适合各种先进应用。在本工作中,首次采用溶液燃烧合成与氢气还原法相结合的方法制备了AlO/Cu复合粉末(ACCP),随后采用放电等离子烧结(SPS)技术制备了ACCM。详细研究了AlO含量和SPS温度对ACCM性能(相对密度、硬度、摩擦系数和电导率等)的影响。结果表明,ACCM非常致密,其微观结构由均匀分布在Cu基体中的细小AlO颗粒组成。随着SPS温度的升高,ACCM的相对密度和硬度先增加后降低。在775℃时,相对密度和硬度分别达到最大值98.19%和121.4 HV。随着AlO含量的增加,尽管ACCM的相对密度逐渐降低,但其摩擦系数却增加了。此外,随着AlO含量的增加,ACCM的硬度先增加后降低,在添加量为3 wt.%时达到最大值(121.4 HV)。相反,ACCM的磨损率随着AlO含量的增加先降低后增加,在添加量为3 wt.%时达到最小值(2.32×10 mm/(N·m))。