Salzenstein Patrice, Wu Thomas Y
Centre National de la Recherche Scientifique (CNRS), Franche-Comté Electronique Mécanique Thermique Optique Sciences et Technologies (FEMTO-ST) Institute, Université de Franche-Comté (UFC), 25030 Besançon, France.
National Metrology Centre (NMC), Agency for Science, Technology and Research (A*STAR), 8 CleanTech Loop, #01-20, Singapore 637145, Singapore.
Micromachines (Basel). 2023 Jul 15;14(7):1429. doi: 10.3390/mi14071429.
The expanded uncertainty of the measured Brillouin scattering shift frequencies is essential in assessing the measurements of parameters of various materials. We describe the general operation principles of a Brillouin light scattering (BLS) spectrometer with a high-power laser and a scanning tandem Fabry-Pérot interferometer (TFPI) for material characterization. Various uncertainty components have been analyzed for the BLS spectrometer following the Guide to the Expression of Uncertainty in Measurement (GUM). The expanded relative uncertainty in the measured Brillouin frequency shift of 15.70 GHz for polymethyl methacrylate (PMMA) was estimated to be 0.26%. The calculated Brillouin frequency shift (based on material properties of PMMA) was determined to be 15.44 GHz with expanded relative uncertainty of 2.13%. It was shown that the measured and calculated Brillouin frequency shifts for PMMA agree within their expanded uncertainties. The TFPI-based BLS spectrometer can be used to measure the longitudinal modulus of materials with an expanded uncertainty of 1.9%, which is smaller than that of the ultrasonic velocity-based method (estimated to be 2.9%).
测量的布里渊散射频移的扩展不确定度对于评估各种材料参数的测量至关重要。我们描述了一种用于材料表征的具有高功率激光器和扫描串联法布里 - 珀罗干涉仪(TFPI)的布里渊光散射(BLS)光谱仪的一般工作原理。按照《测量不确定度表示指南》(GUM)对BLS光谱仪的各种不确定度分量进行了分析。聚甲基丙烯酸甲酯(PMMA)测量的布里渊频移为15.70 GHz时,扩展相对不确定度估计为0.26%。基于PMMA材料特性计算的布里渊频移确定为15.44 GHz,扩展相对不确定度为2.13%。结果表明,PMMA测量的和计算的布里渊频移在其扩展不确定度范围内相符。基于TFPI的BLS光谱仪可用于测量材料的纵向模量,扩展不确定度为1.9%,小于基于超声速度的方法(估计为2.9%)。