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基于顶空固相微萃取-气相色谱-质谱联用技术的七种芥末酱挥发性风味化合物的比较分析

Comparative Analysis of Volatile Flavor Compounds in Seven Mustard Pastes via HS-SPME-GC-MS.

作者信息

Liang Miao, Wang Rui, Wu Yajian, Xin Runhu, Guan Wei, Liu Yuping

机构信息

China Food Flavor and Nutrition Health Innovation Center, Beijing Technology and Business University, Beijing 100048, China.

School of Light Industry, Beijing Technology & Business University, Beijing 100048, China.

出版信息

Molecules. 2023 Jul 18;28(14):5482. doi: 10.3390/molecules28145482.

DOI:10.3390/molecules28145482
PMID:37513353
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10383883/
Abstract

To identify the volatile flavor components in mustard paste (MP), the volatile compounds in seven MPs available on the market were isolated and analyzed by headspace solid-phase microextraction combined with gas chromatography-mass spectrometry. A total of 27 volatile constituents were found by mass spectra and retention index compared to the data obtained from reference compounds or the related literature and databases; these compounds included nine esters, three sulfur-containing compounds, two nitriles, three ketones, three alkenes, and seven other compounds. Of the 27 compounds, 6 compounds came from the turmeric added to MPs. Among the components detected, some compounds derived from AITC were allyl thiocyanate, carbon disulfide, allyl mercaptan, diallyl sulfide, and diallyl disulfide. The results obtained provide a better and comprehensive recognition of the volatile flavor compounds in MPs, and have some reference values for developing and applying isothiocyanate compounds.

摘要

为鉴定芥末酱(MP)中的挥发性风味成分,采用顶空固相微萃取结合气相色谱 - 质谱联用技术,对市售7种芥末酱中的挥发性化合物进行了分离和分析。通过质谱和保留指数,并与参考化合物或相关文献及数据库中的数据进行比较,共鉴定出27种挥发性成分;这些化合物包括9种酯类、3种含硫化合物、2种腈类、3种酮类、3种烯烃类和7种其他化合物。在这27种化合物中,有6种化合物来自添加到芥末酱中的姜黄。在检测到的成分中,一些源自异硫氰酸烯丙酯(AITC)的化合物有烯丙基硫氰酸盐、二硫化碳、烯丙基硫醇、二烯丙基硫醚和二烯丙基二硫醚。所得结果能更好、更全面地认识芥末酱中的挥发性风味化合物,对异硫氰酸酯类化合物的开发和应用具有一定参考价值。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0511/10383883/2c3bb03e3f59/molecules-28-05482-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0511/10383883/c9134b14fa16/molecules-28-05482-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0511/10383883/f67568a79d77/molecules-28-05482-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0511/10383883/2c3bb03e3f59/molecules-28-05482-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0511/10383883/c9134b14fa16/molecules-28-05482-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0511/10383883/f67568a79d77/molecules-28-05482-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0511/10383883/2c3bb03e3f59/molecules-28-05482-g003.jpg

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本文引用的文献

1
Important Odorants of Four Brassicaceae Species, and Discrepancies between Glucosinolate Profiles and Observed Hydrolysis Products.四种十字花科植物的重要气味物质,以及硫代葡萄糖苷谱与观察到的水解产物之间的差异
Foods. 2021 May 11;10(5):1055. doi: 10.3390/foods10051055.
2
Antibacterial activity and main action pathway of benzyl isothiocyanate extracted from papaya seeds.从木瓜籽中提取的苄基异硫氰酸酯的抗菌活性及其主要作用途径。
J Food Sci. 2021 Jan;86(1):169-176. doi: 10.1111/1750-3841.15539. Epub 2020 Dec 9.
3
An Integrated Metabolomics Study of Glucosinolate Metabolism in Different Brassicaceae Genera.
不同十字花科属中硫代葡萄糖苷代谢的综合代谢组学研究
Metabolites. 2020 Jul 31;10(8):313. doi: 10.3390/metabo10080313.
4
Chemodiversity of the Glucosinolate-Myrosinase System at the Single Cell Type Resolution.单细胞类型分辨率下硫代葡萄糖苷-黑芥子酶系统的化学多样性
Front Plant Sci. 2019 May 21;10:618. doi: 10.3389/fpls.2019.00618. eCollection 2019.
5
Reactivity and stability of selected flavor compounds.所选风味化合物的反应性和稳定性。
J Food Drug Anal. 2015 Jun;23(2):176-190. doi: 10.1016/j.jfda.2015.02.001. Epub 2015 Mar 28.
6
Antimicrobial Packaging for Extending the Shelf Life of Bread-A Review.抗菌包装延长面包货架期的研究进展。
Crit Rev Food Sci Nutr. 2016 Jun 10;56(8):1313-24. doi: 10.1080/10408398.2013.768198.
7
Enhancement of aqueous stability of allyl isothiocyanate using nanoemulsions prepared by an emulsion inversion point method.采用反相乳液法制备纳米乳液提高丙烯基异硫氰酸酯的水分散稳定性。
J Colloid Interface Sci. 2015 Jan 15;438:130-137. doi: 10.1016/j.jcis.2014.09.055. Epub 2014 Sep 30.
8
Various concentrations of erucic acid in mustard oil and mustard.芥籽油和芥菜中不同浓度的芥酸。
Food Chem. 2014 Jun 15;153:393-7. doi: 10.1016/j.foodchem.2013.12.073. Epub 2013 Dec 28.
9
Glucosinolate degradation products, isothiocyanates, nitriles, and thiocyanates, induce stomatal closure accompanied by peroxidase-mediated reactive oxygen species production in Arabidopsis thaliana.硫代葡萄糖苷降解产物、异硫氰酸酯、腈类和硫氰酸盐会诱导拟南芥气孔关闭,并伴随着过氧化物酶介导的活性氧生成。
Biosci Biotechnol Biochem. 2013;77(5):977-83. doi: 10.1271/bbb.120928. Epub 2013 May 7.
10
Comparison of simultaneous distillation extraction and solid-phase microextraction for the determination of volatile flavor components.
J Chromatogr A. 2001 Sep 28;930(1-2):1-7. doi: 10.1016/s0021-9673(01)01187-6.