Takahashi Yukio, Abe Masaki, Uematsu Hideshi, Takazawa Shuntaro, Sasaki Yuhei, Ishiguro Nozomu, Ozaki Kyosuke, Honjo Yoshiaki, Nishino Haruki, Kobayashi Kazuo, Hiraki Toshiyuki Nishiyama, Joti Yasumasa, Hatsui Takaki
Institute of Multidisciplinary Research for Advanced Materials (IMRAM), Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577, Japan.
International Center for Synchrotron Radiation Innovation Smart (SRIS), Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577, Japan.
J Synchrotron Radiat. 2023 Sep 1;30(Pt 5):989-994. doi: 10.1107/S1600577523004897. Epub 2023 Aug 1.
Ptychographic coherent diffraction imaging (PCDI) is a synchrotron X-ray microscopy technique that provides high spatial resolution and a wide field of view. To improve the performance of PCDI, the performance of the synchrotron radiation source and imaging detector should be improved. In this study, ptychographic diffraction pattern measurements using the CITIUS high-speed X-ray image detector and the corresponding image reconstruction are reported. X-rays with an energy of 6.5 keV were focused by total reflection focusing mirrors, and a flux of ∼2.6 × 10 photons s was obtained at the sample plane. Diffraction intensity data were collected at up to ∼250 Mcounts s pixel without saturation of the detector. Measurements of tantalum test charts and silica particles and the reconstruction of phase images were performed. A resolution of ∼10 nm and a phase sensitivity of ∼0.01 rad were obtained. The CITIUS detector can be applied to the PCDI observation of various samples using low-emittance synchrotron radiation sources and to the stability evaluation of light sources.
叠层相干衍射成像(PCDI)是一种同步辐射X射线显微镜技术,可提供高空间分辨率和宽视场。为了提高PCDI的性能,应提高同步辐射源和成像探测器的性能。在本研究中,报告了使用CITIUS高速X射线图像探测器进行的叠层衍射图案测量及相应的图像重建。能量为6.5 keV的X射线通过全反射聚焦镜聚焦,在样品平面处获得了约2.6×10 光子/秒的通量。在探测器不饱和的情况下,以高达约250 兆计数/秒/像素的速度收集衍射强度数据。进行了钽测试图和二氧化硅颗粒的测量以及相位图像的重建。获得了约10 nm的分辨率和约0.01 rad的相位灵敏度。CITIUS探测器可应用于使用低发射度同步辐射源对各种样品进行PCDI观察以及光源的稳定性评估。