Nirala A, Soren S, Kumar Navneet, Khan Mohammad Amir, Islam Saiful, Khan Nadeem A
Department of Fuel, Minerals and Metallurgical Engineering, Indian Institute of Technology (ISM) Dhanbad, Dhanbad, India.
Department of Mechanical Engineering, Galgotias College of Engineering and Technology, Greater Noida, India.
Sci Rep. 2023 Aug 12;13(1):13147. doi: 10.1038/s41598-023-39713-2.
The aluminum nanocomposite is fabricated through squeeze stir casting method where CNT, SiC/BC powder has been used as a reinforcement in an aluminum matrix. Squeeze action in stir casting opted due to proper reinforcement of 2 vol% of CNT in the matrix. The boron carbide and silicon carbide have been added by 8 and 12 vol% in the matrix. Uniform distribution of reinforcement and phase analysis has been shown by scanning electron microscopy (SEM) and XRD analysis. The formation of intermetallic compounds like AlBC and AlC, dislocation forests, and the interaction of the reinforcement with the matrix are all confirmed by transmission electron microscopy (TEM). The micro-mechanical behavior of aluminum nanocomposites was investigated using nano indentation. The nano hardness, Vickers hardness, and Young's modulus of 12 vol% BC compared with 12 vol% of SiC are increased by 12%, 23%, and 16%, respectively, and the same trend has been observed for the 8 vol% BC reinforced composite. The model analysis for Young's modulus has been done and the experimental value for the modulus of elasticity of the composite are validated and not find such differences significantly. The surface topography was determined, furrow scratches and wear scars, and it was discovered that BC reinforced composites have reduced stripping pits inside the wear marks, as well as lower wear width and depth. Wear analysis is essential because abrasive encounters result in substantial damage owing to larger pits and bigger wear scars.
铝基纳米复合材料是通过挤压搅拌铸造法制备的,其中碳纳米管(CNT)、碳化硅/硼化碳(SiC/BC)粉末被用作铝基体中的增强材料。由于在基体中适当增强了2体积%的碳纳米管,所以选择了搅拌铸造中的挤压操作。在基体中添加了8体积%和12体积%的碳化硼和碳化硅。通过扫描电子显微镜(SEM)和X射线衍射(XRD)分析显示了增强材料的均匀分布和相分析。通过透射电子显微镜(TEM)证实了金属间化合物如AlBC和AlC的形成、位错林以及增强材料与基体的相互作用。使用纳米压痕研究了铝基纳米复合材料的微观力学行为。与12体积%的碳化硅相比,12体积%的硼化碳增强复合材料的纳米硬度、维氏硬度和杨氏模量分别提高了12%、23%和16%,对于8体积%的硼化碳增强复合材料也观察到了相同的趋势。对杨氏模量进行了模型分析,复合材料弹性模量的实验值得到了验证,且未发现明显差异。测定了表面形貌、犁沟划痕和磨损疤痕,发现硼化碳增强复合材料在磨损痕迹内的剥落坑减少,磨损宽度和深度也较低。磨损分析至关重要,因为磨料接触会由于较大的凹坑和较大的磨损疤痕而导致严重损坏。