Mostafa Wageha A, Elshanawany Soad A, Otaif Khadejah D, Khalifa Mona, Elgazzar Elsayed
Entomolgy Section, Zoology Department, Faculty of Science, Zagazig University, Zagazig, Egypt.
Physics Department, Jazan University, 86736, Jazan, Saudi Arabia.
BMC Chem. 2024 Jan 12;18(1):11. doi: 10.1186/s13065-023-01108-9.
Zinc chromium oxide (Cr/ZnO, 5wt.%) was prepared by a facile chemical co-precipitation route. The structure, composition, and chemical bonding were analyzed using X-ray diffraction (XRD), Energy dispersive X-ray spectroscopy (EDX), and Fourier-transform infrared spectroscopy (FTIR) indicating that chromium ions were integrated the host framework to form Cr/ZnO nanocomposite. Scanning electron microscopy (SEM) and Transmission electron microscopy (TEM) micrographs showed comb-shaped nanoparticles with an average size 20 nm and large surface area. The energy gap of the thin films was estimated from T% and R% measurements which exhibit a strong optical absorption edge close to the visible spectrum. The insecticidal activity of the synthesized nanocombs against C. pipiens larvae was evaluated with LC (30.15 ppm) and LC (100.22 ppm). Besides, the nanocomposite showed high antibacterial performance against gram-positive bacteria (Bacillus subtilis) and gram-negative bacteria (Proteus vulgaris) with inhibition zones 21.9 and 19 mm, respectively.
通过简便的化学共沉淀法制备了氧化锌铬(Cr/ZnO,5wt.%)。使用X射线衍射(XRD)、能量色散X射线光谱(EDX)和傅里叶变换红外光谱(FTIR)对其结构、组成和化学键进行了分析,结果表明铬离子融入主体框架形成了Cr/ZnO纳米复合材料。扫描电子显微镜(SEM)和透射电子显微镜(TEM)图像显示为梳状纳米颗粒,平均尺寸为20nm,表面积较大。通过T%和R%测量估算了薄膜的能隙,其显示出靠近可见光谱的强光学吸收边缘。用LC(30.15ppm)和LC(100.22ppm)评估了合成的纳米梳对致倦库蚊幼虫的杀虫活性。此外,该纳米复合材料对革兰氏阳性菌(枯草芽孢杆菌)和革兰氏阴性菌(普通变形杆菌)表现出高抗菌性能,抑菌圈分别为21.9mm和19mm。