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添加银纳米颗粒对正畸粘合剂力学性能的影响。

Effect of the addition of silver nanoparticles on the mechanical properties of an orthodontic adhesive.

作者信息

Sánchez-Tito Marco, Tay Lidia Yileng

机构信息

Facultad de Ciencias de la Salud, Universidad Privada de Tacna, Tacna 23000, Peru.

Facultad de Estomatología, Universidad Peruana Cayetano Heredia, Lima 15102, Peru.

出版信息

Saudi Dent J. 2024 Feb;36(2):359-363. doi: 10.1016/j.sdentj.2023.11.021. Epub 2023 Nov 25.

Abstract

OBJECTIVES

This study evaluated the effects of adding silver nanoparticles on the shear bond strength, microhardness, and surface roughness of orthodontic adhesives.

MATERIAL AND METHODS

Fifty upper premolars were randomly allocated to five groups (n = 10). Orthodontic brackets were bonded with silver nanoparticle (AgNP)-modified adhesives (1 %, 0.5 %, 0.1 %, 0.05 %), and conventional adhesive was used as a control. The shear bond strength was recorded using a universal testing machine, and the adhesive remnant index was evaluated using a stereomicroscope. Ten discs of each adhesive were subjected to the microhardness and surface roughness tests. The Vickers microhardness values were measured under a constant load of 100 g for 30 s using a microhardness tester. The samples were analyzed using a surface profilometer, and the arithmetic average roughness was used as the measurement parameter. Data were analyzed using one-way analysis of variance and chi-square tests. A significance level of 5 % was considered significant.

RESULTS

AgNP concentration > 0.1 % significantly reduced the shear bond strength (p < 0.05). At higher AgNP concentration, the bonding failure pattern occurred mainly at the bracket-resin interface. The Vickers microhardness increased with increasing concentration, and significant differences were observed between the group with 1 % AgNP and the other groups (p < 0.05). The average roughness values were similar between the groups with AgNP concentrations > 0.1 % (p > 0.05).

CONCLUSION

The incorporation of AgNP into an orthodontic adhesive has the potential to decrease the shear bond strength while increasing the microhardness and surface roughness.

摘要

目的

本研究评估添加银纳米颗粒对正畸胶粘剂的剪切粘结强度、显微硬度和表面粗糙度的影响。

材料与方法

将50颗上颌前磨牙随机分为五组(n = 10)。使用银纳米颗粒(AgNP)改性的胶粘剂(1%、0.5%、0.1%、0.05%)粘结正畸托槽,并以传统胶粘剂作为对照。使用万能试验机记录剪切粘结强度,使用体视显微镜评估粘结剂残留指数。对每种胶粘剂的10个圆盘进行显微硬度和表面粗糙度测试。使用显微硬度计在100 g恒定载荷下保持30 s测量维氏显微硬度值。使用表面轮廓仪对样品进行分析,并将算术平均粗糙度用作测量参数。数据采用单因素方差分析和卡方检验进行分析。显著性水平设定为5%。

结果

AgNP浓度>0.1%时显著降低了剪切粘结强度(p < 0.05)。在较高的AgNP浓度下,粘结失败模式主要发生在托槽-树脂界面。维氏显微硬度随浓度增加而升高,1% AgNP组与其他组之间观察到显著差异(p < 0.05)。AgNP浓度>0.1%的组之间平均粗糙度值相似(p > 0.05)。

结论

在正畸胶粘剂中加入AgNP有可能降低剪切粘结强度,同时提高显微硬度和表面粗糙度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b6f2/10897628/24191dfd575a/gr1.jpg

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