Periasamy Kailashbalan, Darouie Maryam, Das Raj, Khatibi Akbar A
School of Engineering, RMIT University, Melbourne, VIC 3000, Australia.
Molecules. 2024 Feb 20;29(5):928. doi: 10.3390/molecules29050928.
In this study, we employed a straightforward flame synthesis process to produce carbon soot containing carbon nano onions (CNOs) using easily accessible ghee oil as a precursor. The ghee oil, with a molecular composition rich in more than 50 carbon atoms, served as an effective source for generating CNOs. The synthesized CNO particles underwent comprehensive characterization through high-resolution transmission electron microscopy (HRTEM), energy dispersive X-ray spectroscopy (EDX), Fourier transform infrared spectroscopy (FTIR), and X-ray diffraction (XRD) analyses, providing a detailed account of their physicochemical properties. In addition, we explored the direct deposition of CNOs on carbon fiber (CF) surfaces for 5 and 10 min via a soot deposition process. The resulting freeze-fracture images obtained from scanning electron microscope (SEM) offered insights into the morphology of the CNO-deposited CF. Our study aims to shed light on the potential applications of CNOs, focusing on their characterization and the possible benefits they may offer in diverse fields, including but not limited to enhancing interfacial bonding in thermoplastic composites.
在本研究中,我们采用了一种简单的火焰合成工艺,以易于获取的酥油为前驱体来制备含碳纳米洋葱(CNOs)的碳烟。酥油的分子组成富含50多个碳原子,是生成CNOs的有效来源。通过高分辨率透射电子显微镜(HRTEM)、能量色散X射线光谱(EDX)、傅里叶变换红外光谱(FTIR)和X射线衍射(XRD)分析对合成的CNO颗粒进行了全面表征,详细说明了它们的物理化学性质。此外,我们通过烟灰沉积工艺探索了将CNOs直接沉积在碳纤维(CF)表面5分钟和10分钟的情况。从扫描电子显微镜(SEM)获得的所得冷冻断裂图像提供了对CNO沉积CF形态的见解。我们的研究旨在阐明CNOs的潜在应用,重点关注其表征以及它们在包括但不限于增强热塑性复合材料界面结合等不同领域可能带来的益处。