Herrmann Stefan, Hirschwald Lukas T, Heidmann Karl H, Linkhorst John, Wessling Matthias
RWTH Aachen University, AVT.CVT - Chair of Chemical Process Engineering, Forckenbeckstr. 51, 52074 Aachen, Germany.
DWI - Leibniz Institute for Interactive Materials, Forckenbeckstr. 50, 52074 Aachen, Germany.
HardwareX. 2023 Dec 20;17:e00506. doi: 10.1016/j.ohx.2023.e00506. eCollection 2024 Mar.
Photocatalytic water treatment is considered a promising technique to prevent micropollutants from entering the environment. However, no off-the-shelf UV reactors on lab scale are available to study new processes and photocatalysts. In this study, we present a tubular UV reactor equipped with 30 UV-LEDs, emitting UV light at 367 nm and a total radiant flux of 42 W. The UV reactor has an irradiated length of 300 mm and can host any transparent chemical reactor on the inside with a maximum diameter of 28 mm. The device is optimized for lab experiments with total dimensions of just 334 mm x 193 mm x 172 mm. Besides water treatment, a broad range of other photochemical and photocatalytic experiments can be performed with the reactor. Two identical UV reactors have been built and are successfully used for photocatalytic water treatment experiments. The degradation of methylene blue with TiO as photocatalyst was studied to validate the UV reactor. Furthermore, photocatalytic and hybrid processes were conducted in the UV reactor to degrade a broad range of pharmaceutical micropollutants.
光催化水处理被认为是一种防止微污染物进入环境的有前景的技术。然而,实验室规模下没有现成的紫外光反应器可用于研究新工艺和光催化剂。在本研究中,我们展示了一种配备30个紫外发光二极管的管式紫外光反应器,其发射波长为367nm的紫外光,总辐射通量为42W。该紫外光反应器的照射长度为300mm,内部可容纳任何最大直径为28mm的透明化学反应器。该装置专为实验室实验而优化,总尺寸仅为334mm×193mm×172mm。除了水处理,该反应器还可用于进行广泛的其他光化学和光催化实验。现已制造了两个相同的紫外光反应器,并成功用于光催化水处理实验。以二氧化钛为光催化剂研究了亚甲基蓝的降解,以验证该紫外光反应器。此外,还在该紫外光反应器中进行了光催化和混合工艺,以降解多种药物微污染物。