Minnesota Dental Research Center for Biomaterials and Biomechanics, School of Dentistry, University of Minnesota, Minneapolis, MN, USA.
Division of Biostatistics, School of Public Health, University of Minnesota, Minneapolis, MN, USA.
Dent Mater. 2024 Jun;40(6):889-896. doi: 10.1016/j.dental.2024.04.005. Epub 2024 Apr 30.
The current study aimed to evaluate the effects of different combinations of chemical and mechanical challenges on the failure load, failure mode and composition of the resulting fracture surfaces of resin-composite restorations.
Three resin composites were used to fill dentin disks (2 mm inner diameter, 5 mm outer diameter, and 2 mm thick) made from bovine incisor roots. The model restorations, half of which were preconditioned with a low-pH buffer (48 h under pH 4.5), were subjected to diametral compression with either a monotonically increasing load (fast fracture) or a cyclic load with a continuously increasing amplitude (accelerated fatigue). The load or number of cycles to failure was noted. SEM was performed on the fracture surfaces to determine the proportions of dentin, adhesive, and resin composite.
Both cyclic fatigue and acid preconditioning significantly reduced the failure load and increased the proportion of interfacial failure in almost all the cases, with cyclic fatigue having a more pronounced effect. Cyclic fatigue also increased the amount of adhesive/hybrid layer present on the fracture surfaces, but the effect of acid preconditioning on the composition of the fracture surfaces varied among the resin composites.
The adhesive or hybrid layer was found to be the least resistant against the chemomechanical challenges among the components forming the model restoration. Increasing such resistance of the tooth-restoration interface, or its ability to combat the bacterial actions that lead to secondary caries following interfacial debonding, can enhance the longevity of resin-composite restorations.
本研究旨在评估不同化学和机械挑战组合对树脂复合材料修复体的失效负荷、失效模式和断裂面成分的影响。
使用三种树脂复合材料填充来自牛切牙根的牙本质圆盘(内径 2mm,外径 5mm,厚 2mm)。模型修复体的一半用低 pH 值缓冲液预处理(pH4.5 下 48h),然后进行直径压缩,要么是单调递增的负荷(快速断裂),要么是负荷幅值连续增加的循环负荷(加速疲劳)。记录失效时的负荷或循环次数。在断裂面上进行 SEM 分析,以确定牙本质、粘结剂和树脂复合材料的比例。
循环疲劳和酸预处理都显著降低了失效负荷,并增加了几乎所有情况下的界面失效比例,其中循环疲劳的影响更为显著。循环疲劳还增加了断裂面上的粘结/混合层的量,但酸预处理对断裂面成分的影响因树脂复合材料而异。
在构成模型修复体的各组成部分中,粘结剂或混合层被发现是最不耐受化学机械挑战的。增加牙体修复界面的这种抵抗力,或其在界面脱粘后抵抗导致继发龋的细菌作用的能力,可以提高树脂复合材料修复体的耐久性。