Braig Christoph, Probst Jürgen, Löchel Heike, Pina Ladislav, Krist Thomas, Seifert Christian
Institute of Applied Photonics e.V., Rudower Chaussee 29/31, 12489 Berlin, Germany.
NOB Nano Optics Berlin GmbH, Krumme Straße 64, 10627 Berlin, Germany.
J Synchrotron Radiat. 2024 Jul 1;31(Pt 4):690-697. doi: 10.1107/S1600577524003643. Epub 2024 Jun 6.
A reliable `in situ' method for wavefront sensing in the soft X-ray domain is reported, developed for the characterization of rotationally symmetric optical elements, like an ellipsoidal mirror shell. In a laboratory setup, the mirror sample is irradiated by an electron-excited (4.4 keV), micrometre-sized (∼2 µm) fluorescence source (carbon K, 277 eV). Substantially, the three-dimensional intensity distribution I(r) is recorded by a CCD camera (2048 × 512 pixels of 13.5 µm) at two positions along the optical axis, symmetrically displaced by ±21-25% from the focus. The transport-of-intensity equation is interpreted in a geometrical sense from plane to plane and implemented as a ray tracing code, to retrieve the phase Φ(r) from the radial intensity gradient on a sub-pixel scale. For reasons of statistical reliability, five intra-/extra-focal CCD image pairs are evaluated and averaged to an annular two-dimensional map of the wavefront error {\cal W}. In units of the test wavelength (C K), an r.m.s. value \sigma_{\cal{W}} = ±10.9λ and a peak-to-valley amplitude of ±31.3λ are obtained. By means of the wavefront, the focus is first reconstructed with a result for its diameter of 38.4 µm, close to the direct experimental observation of 39.4 µm (FWHM). Secondly, figure and slope errors of the ellipsoid are characterized with an average of ±1.14 µm and ±8.8 arcsec (r.m.s.), respectively, the latter in reasonable agreement with the measured focal intensity distribution. The findings enable, amongst others, the precise alignment of axisymmetric X-ray mirrors or the design of a wavefront corrector for high-resolution X-ray science.
报道了一种用于软X射线领域波前传感的可靠“原位”方法,该方法是为表征旋转对称光学元件(如椭球镜壳)而开发的。在实验室装置中,镜样品由电子激发(4.4 keV)、微米级(约2 µm)的荧光源(碳K,277 eV)照射。实质上,三维强度分布I(r)由电荷耦合器件相机(2048×512像素,像素尺寸为13.5 µm)在沿光轴的两个位置记录,这两个位置相对于焦点对称地偏移±21 - 25%。强度传输方程从几何意义上在平面之间进行解释,并实现为光线追踪代码,以便在亚像素尺度上从径向强度梯度中检索相位Φ(r)。出于统计可靠性的原因,对五对焦内/焦外电荷耦合器件图像对进行评估并平均,得到波前误差{\cal W}的环形二维图。以测试波长(碳K)为单位,获得均方根值\sigma_{\cal{W}} = ±10.9λ和峰谷幅度±31.3λ。借助波前,首先重建焦点,其直径结果为38.4 µm,接近直接实验观测值39.4 µm(半高宽)。其次,椭球的形状和斜率误差分别表征为平均±1.14 µm和±8.8弧秒(均方根),后者与测量的焦强度分布合理吻合。这些发现尤其能够实现轴对称X射线镜的精确对准或用于高分辨率X射线科学的波前校正器的设计。