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基于激光功率、扫描速度和铺粉间距最佳工艺参数的低SiC体积分数和高SiC体积分数增材制造SiC/Ti6Al4V(ELI)复合材料的对比分析

A Comparative Analysis of Low and High SiC Volume Fraction Additively Manufactured SiC/Ti6Al4V(ELI) Composites Based on the Best Process Parameters of Laser Power, Scanning Speed and Hatch Distance.

作者信息

Thamae Masenate, Maringa Maina, du Preez Willie

机构信息

Department of Mechanical and Mechatronics Engineering, Faculty of Engineering, Built Environment and Information Technology, Central University of Technology, Bloemfontein 9301, Free State, South Africa.

Centre for Rapid Prototyping and Manufacturing, Faculty of Engineering, Built Environment and Information Technology, Central University of Technology, Bloemfontein 9301, Free State, South Africa.

出版信息

Materials (Basel). 2024 May 28;17(11):2606. doi: 10.3390/ma17112606.

Abstract

Silicon carbide (SiC) exhibits intriguing thermo-physical properties such as higher heat capacity and conductivity, as well as a lower density than Ti6Al4V(ELI). These properties make SiC a good candidate for the reinforcement of Ti6Al4V(ELI) with respect to its use as a heat shield in aero turbines to increase their efficiency. The traditional materials used in aircraft structures were required to have a combination of good mechanical properties such as strength, stiffness, and hardness and low weight, as well as low thermo-physical properties such as coefficient of thermal expansion (CTE) and thermal conductivity. The alloy Ti6Al4V(ELI) has a density of 4.45 g/cm, which is lower than that of structural steel (7.4 g/cm) and higher than that of aluminium (2.5 g/cm). Lower density benefits light weighting. Aluminium is the lightest of the traditional materials used but has relatively low strength. The CTE of SiC of 4.6 × 10/K is lower than that of Ti6Al4V(ELI) of 8.6 × 10/K, while the density of SiC of 3.21 g/cm is lower than that of Ti6Al4V(ELI) of 4.45 g/cm. Therefore, from the theory of composites, SiC/Ti6Al4V(ELI) composites are expected to have lower densities and CTEs than those of Ti6Al4V(ELI), thus providing for lightweighting and less thermal related buckling or separation at their joints with carbon/epoxy resin panels. The specific strength, stiffness, and Knoop hardness of SiC of 75-490 kNm/kg, 132 MNm/kg, and 600-3800 GPa, respectively, are generally larger than those of Ti6Al4V(ELI) of 211 KNm/kg, 24 MNm/kg, and 880 GPa, respectively. Therefore, investigating reinforcement of Ti6Al4V(ELI) with SiC particles is worthwhile as it will lead to the formation of composites that are stronger, stiffer, harder, and lighter, with lower values of CTE. For additive manufacturing, this requires initial studies to optimise the process parameters of laser power and scanning speed for single tracks. To print single tracks in the present work, different laser powers ranging from 100 W to 350 W and scanning speeds ranging from 0.3 m/s to 2.7 m/s were used for different SiC volume fraction values of values. To print single layers, different values of hatch distance were used together with the best values of laser power and scanning speed determined elsewhere by the authors for different volume fractions of SiC. Through optical microscopy, the built tracks and their cross sections were examined. By using laser power and scanning speeds of 200 W and 1.2 m/s, and 150 W and 0.8 m/s, respectively, the best tracks at 5% and 10% volume fractions were obtained, whereas the best tracks at 25% volume fraction were achieved using a laser power of 200 W and a scanning speed of 0.5 m/s. Furthermore, the results showed that the maximum SiC volume percentage of 30% resulted in limited or no penetration. Therefore, it is concluded from the study that parts with improved mechanical properties can be produced at SiC volume fractions ranging from 5% to 25%, while parts produced at the high volume fraction of 30% would have unacceptable mechanical qualities for the final part.

摘要

碳化硅(SiC)具有引人关注的热物理性能,如较高的热容量和热导率,且密度低于Ti6Al4V(ELI)。这些特性使SiC成为增强Ti6Al4V(ELI)的理想候选材料,可用于航空涡轮机的隔热罩以提高其效率。飞机结构中使用的传统材料需要具备强度、刚度和硬度等良好机械性能与低重量的组合,以及低热膨胀系数(CTE)和热导率等低热物理性能。合金Ti6Al4V(ELI)的密度为4.45 g/cm³,低于结构钢(7.4 g/cm³)且高于铝(2.5 g/cm³)。较低的密度有利于减轻重量。铝是所用传统材料中最轻的,但强度相对较低。SiC的CTE为4.6×10⁻⁶/K,低于Ti6Al4V(ELI)的8.6×10⁻⁶/K,而SiC的密度为3.21 g/cm³,低于Ti6Al4V(ELI)的4.45 g/cm³。因此,从复合材料理论来看,预计SiC/Ti6Al4V(ELI)复合材料的密度和CTE低于Ti6Al4V(ELI),从而实现轻量化,并减少其与碳/环氧树脂面板连接处因热相关的屈曲或分离。SiC的比强度、比刚度和努氏硬度分别为75 - 490 kNm/kg、132 MNm/kg和600 - 3800 GPa,通常分别大于Ti6Al4V(ELI)的211 KNm/kg、24 MNm/kg和880 GPa。因此,研究用SiC颗粒增强Ti6Al4V(ELI)是值得的,因为这将形成更强、更硬、更轻且CTE值更低的复合材料。对于增材制造,这需要进行初步研究以优化单道激光功率和扫描速度等工艺参数。在本工作中为打印单道,针对不同的SiC体积分数值,使用了100 W至350 W的不同激光功率以及0.3 m/s至2.7 m/s的扫描速度。为打印单层,使用了不同的填充间距值以及作者在其他地方针对不同SiC体积分数确定的最佳激光功率和扫描速度值。通过光学显微镜检查了构建的轨迹及其横截面。分别使用200 W和1.2 m/s以及150 W和0.8 m/s的激光功率和扫描速度,在5%和10%体积分数下获得了最佳轨迹,而在25%体积分数下使用200 W的激光功率和0.5 m/s的扫描速度获得了最佳轨迹。此外,结果表明,30%的最大SiC体积百分比导致有限的穿透或无穿透。因此,从该研究得出结论,在SiC体积分数为5%至25%的范围内可以生产出机械性能得到改善的零件,而在30%的高体积分数下生产的零件对于最终零件将具有不可接受的机械质量。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1821/11173544/2230f1f5e74e/materials-17-02606-g001.jpg

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