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通过X射线微分析为高级定制剪裁阻挡层设计：见解与指南

Tailoring barrier layers design for haute couture through X-ray microanalysis: Insights and guidelines.

作者信息

Biffoli Fabio, Giurlani Walter, Vorobyova Mariya, Maccioni Irene, Giovani Claudia, Salvi Manuel, Cianfanelli Elisabetta, Pagliai Marco, Innocenti Massimo

机构信息

Department of Chemistry "Ugo Schiff", University of Florence, Via della Lastruccia 3, 50019, Sesto Fiorentino (FI), Italy.

Materia Firenze Lab s.r.l., Gruppo Materia Firenze, Via delle Fonti 8/E, 50018, Scandicci (FI), Italy.

出版信息

Heliyon. 2024 Jun 1;10(11):e32147. doi: 10.1016/j.heliyon.2024.e32147. eCollection 2024 Jun 15.

DOI:10.1016/j.heliyon.2024.e32147
PMID:38947480
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11214454/
Abstract

Barrier layers against intermetallic diffusion are a fundamental part on engineering electroplated coatings as they improve the lifetime of goods reducing wastes and improving the sustainability of the production chain. This study aims to set a cost-effective methodology to characterize barrier systems by evaluating the effectiveness with a recent approach based on XRF and EDS and characterize the kinetic of diffusion processes with X-ray diffractometry. Several high fashion barrier systems were tested highlighting that anticorrosion systems are not automatically suited as barrier layers for intermetallic diffusion, as opposed to industrial practice. Investigations on gold coatings obtained varying the current density revealed a correlation between the activation energy of the diffusion process, roughness, and crystallite size.

摘要

防止金属间扩散的阻挡层是工程电镀涂层的基本组成部分，因为它们可以延长产品寿命，减少浪费并提高生产链的可持续性。本研究旨在建立一种经济高效的方法，通过基于XRF和EDS的最新方法评估其有效性来表征阻挡系统，并利用X射线衍射法表征扩散过程的动力学。测试了几种高级时尚的阻挡系统，结果表明，与工业实践相反，防腐系统并非自动适用于金属间扩散的阻挡层。对通过改变电流密度获得的金涂层的研究揭示了扩散过程的活化能、粗糙度和微晶尺寸之间的相关性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/68c1c79011db/gr9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/67d48fcf843a/ga1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/328956736b3b/gr1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/3a2c731fcc3f/gr2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/3a359cfa3be2/gr3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/f3f6aa8552ae/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/0b55ed18a45d/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/baaf44ea619d/gr6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/ec5c63e3ada4/gr7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/b01eceb18911/gr8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/68c1c79011db/gr9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/67d48fcf843a/ga1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/328956736b3b/gr1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/3a2c731fcc3f/gr2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/3a359cfa3be2/gr3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/f3f6aa8552ae/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/0b55ed18a45d/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/baaf44ea619d/gr6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/ec5c63e3ada4/gr7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/b01eceb18911/gr8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/467d/11214454/68c1c79011db/gr9.jpg

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