Department of Agricultural and Biosystems Engineering, Faculty of Agriculture, Benha University, 13736 Moshtohor, Toukh, Egypt; Department of Food Technology, Faculty of Science, Chulalongkorn University, Bangkok 10330, Thailand.
Department of Food Technology, Faculty of Science, Chulalongkorn University, Bangkok 10330, Thailand.
Ultrason Sonochem. 2024 Aug;108:106949. doi: 10.1016/j.ultsonch.2024.106949. Epub 2024 Jun 21.
Investigating the extraction of bioactive compounds represents a hopeful direction for maximizing the value of longan fruit byproducts. This study explored the influence of ultrasonic-assisted extraction (UAE) parameters-specifically ultrasonic power ratios, temperatures, and exposure times-utilizing water as a green solvent on several properties of the longan seeds extract (LSE). These properties encompassed the energy consumption of the UAE process (EC), extraction yield (EY), total phenolic contents (TPC), total flavonoid contents (TFC), and antioxidant activity (DPPH). Additionally, the study sought to optimize the conditions of UAE process and examine its thermodynamic properties. A three-level, three-factor full factorial design was utilized to assess the effects of different factors on LSE properties. Results indicated that EC, EY, TPC, TFC, and DPPH were significantly influenced by power ratios, temperatures, and exposure time. Moreover, the proposed models effectively characterized the variations in different properties during the extraction process. The optimized extraction conditions, aimed at minimizing EC while maximizing EY, TPC, TFC, and DPPH radical scavenging activity, were demonstrated as an ultrasonic power ratio of 44.4 %, a temperature of 60 °C, and an extraction time of 17.7 min. Optimization led to 563 kJ for EC, 7.85 % for EY, 47.21 mg GAE/mL for TPC, 96.8 mg QE/mL for TFC, and 50.15 % for DPPH radical scavenging activity. The results emphasized that the UAE process exhibited characteristics of endothermicity and spontaneity. The results provide valuable insights that could inform the enhancement of extraction processes, potentially benefiting industrial utilization and pharmaceutical formulations.
研究生物活性化合物的提取代表了最大限度地提高龙眼果实副产物价值的一个有希望的方向。本研究探讨了超声辅助提取 (UAE) 参数——特别是超声功率比、温度和暴露时间——利用水作为绿色溶剂对龙眼种子提取物 (LSE) 的几个性质的影响。这些性质包括 UAE 过程的能量消耗 (EC)、提取产率 (EY)、总酚含量 (TPC)、总黄酮含量 (TFC) 和抗氧化活性 (DPPH)。此外,该研究旨在优化 UAE 过程的条件并研究其热力学性质。采用三水平三因素完全析因设计评估不同因素对 LSE 性质的影响。结果表明,EC、EY、TPC、TFC 和 DPPH 受到功率比、温度和暴露时间的显著影响。此外,所提出的模型有效地描述了提取过程中不同性质的变化。优化的提取条件旨在最小化 EC 同时最大化 EY、TPC、TFC 和 DPPH 自由基清除活性,结果表明超声功率比为 44.4%、温度为 60°C 和提取时间为 17.7 分钟。优化后 EC 为 563kJ,EY 为 7.85%,TPC 为 47.21mgGAE/mL,TFC 为 96.8mgQE/mL,DPPH 自由基清除活性为 50.15%。结果强调了 UAE 过程表现出吸热和自发性的特点。研究结果提供了有价值的见解,可为提取过程的增强提供信息,可能有利于工业利用和药物制剂。