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石墨烯-聚酰胺6复合材料的机械性能和抗菌性能

Mechanical and Antimicrobial Properties of the Graphene-Polyamide 6 Composite.

作者信息

Głuchowski Paweł, Macieja Marta, Tomala Robert, Stefanski Mariusz, Stręk Wiesław, Ptak Maciej, Szymański Damian, Szustakiewicz Konrad, Junka Adam, Dudek Bartłomiej

机构信息

Institute of Low Temperature and Structure Research Polish Academy of Sciences, PL-50422 Wroclaw, Poland.

Faculty of Chemistry, Wroclaw University of Science and Technology, PL-50370 Wroclaw, Poland.

出版信息

Materials (Basel). 2024 Jul 12;17(14):3465. doi: 10.3390/ma17143465.

Abstract

This paper presents the synthesis and characterization of graphene-polymer composites, focusing on their mechanical and antibacterial properties. Graphene flakes were obtained via an electrochemical method and integrated into polyamide 6 (PA6) matrices using melt intercalation. Various characterization techniques confirmed the quality of the graphene flakes, including X-ray diffraction (XRD), Raman spectroscopy, and infrared (IR) spectroscopy, as well as scanning and transmission electron microscopy (SEM and TEM) imaging. Mechanical tests showed an increase in the elastic modulus with graphene incorporation, while the impact strength decreased. The SEM analysis highlighted the dispersion of the graphene flakes within the composites and their impact on fracture behavior. Antimicrobial tests demonstrated significant antibacterial properties of the composites, attributed to both oxidative stress and mechanical damage induced by the graphene flakes. The results suggest promising applications for graphene-polymer composites in advanced antimicrobial materials.

摘要

本文介绍了石墨烯-聚合物复合材料的合成与表征,重点关注其机械性能和抗菌性能。通过电化学方法获得石墨烯薄片,并采用熔体插层法将其整合到聚酰胺6(PA6)基体中。各种表征技术证实了石墨烯薄片的质量,包括X射线衍射(XRD)、拉曼光谱、红外(IR)光谱,以及扫描和透射电子显微镜(SEM和TEM)成像。力学测试表明,加入石墨烯后弹性模量增加,而冲击强度降低。SEM分析突出了石墨烯薄片在复合材料中的分散情况及其对断裂行为的影响。抗菌测试表明复合材料具有显著的抗菌性能,这归因于石墨烯薄片引起的氧化应激和机械损伤。结果表明石墨烯-聚合物复合材料在先进抗菌材料方面具有广阔的应用前景。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/64a7/11278109/ff9bdb686ba2/materials-17-03465-g001.jpg

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