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新型计算机辅助设计和计算机辅助制造树脂基冠材料与聚醚醚酮和钛的粘结强度。

Bond strength of recently introduced computer-aided design and computer-aided manufacturing resin-based crown materials to polyetheretherketone and titanium.

机构信息

Associate Professor, Department of Prosthodontics, Faculty of Dentistry, Ordu University, Ordu, Turkey.

Associate Professor, Department of Prosthodontics, Faculty of Dentistry, Biruni University, Istanbul, Turkey; and ITI Scholar, Department of Reconstructive Dentistry and Gerodontology, School of Dental Medicine, University of Bern, Bern, Switzerland.

出版信息

J Prosthet Dent. 2024 Nov;132(5):1066.e1-1066.e8. doi: 10.1016/j.prosdent.2024.07.019. Epub 2024 Aug 2.

Abstract

STATEMENT OF PROBLEM

Several additively and subtractively manufactured resin-based materials indicated for interim and definitive fixed dental prostheses have been launched. However, knowledge of the bond strength of these materials to different implant abutment materials is limited.

PURPOSE

The purpose of this in vitro study was to evaluate the shear bond strength (SBS) of additively and subtractively manufactured resin-based materials to different implant abutment materials.

MATERIAL AND METHODS

One hundred and ten disk-shaped specimens (Ø3×3 mm) were fabricated either additively from 2 resins indicated for definitive use (Crowntec; AM_CT and VarseoSmile Crown Plus; AM_VS) and 1 resin indicated for interim use (FREEPRINT temp; AM_FP) or subtractively from a nanographene-reinforced polymethyl methacrylate (G-CAM; SM_GC) and a high-impact polymer composite (breCAM.HIPC; SM_BC). After allocating 2 specimens from each group for scanning electron microscope evaluation, the specimens were divided according to the abutment material (CopraPeek; polyetheretherketone, PEEK and Dentium Superline Pre-Milled Abutment; titanium, Ti) (n=10). All specimens were airborne-particle abraded with 50-µm aluminum oxide. After applying a resin primer (Visio.link) to PEEK and an adhesive primer (Clearfil Ceramic Primer Plus) to Ti specimens, a self-adhesive resin cement (PANAVIA SA Cement Universal) was used for cementation. All specimens were stored in distilled water (24 hours, 37 °C), and a universal testing device was used for the SBS test. SBS data were analyzed with 2-way analysis of variance and Tukey honestly significant difference tests, while the chi-squared test was used to evaluate the difference among the abutment-resin pairs in terms of failure modes (α=.05).

RESULTS

The interaction between the material type and the abutment type and the main factor of material type affected the SBS (P<.001). SM_BC-PEEK and SM_GC had the lowest SBS followed by SM_BC-Ti, whereas AM_VS-PEEK had the highest SBS (P≤.001). AM_CT-Ti had higher SBS than AM_FP-PEEK (P=.026). SM_GC had the lowest and AM_VS had the highest SBS, while AM_CT and AM_FP had higher SBS than SM_BC (P≤.004). The distribution of failure modes was significantly different among tested material-abutment pairs, and only for AM_CT among tested materials (P≤.025). Most of the material-abutment pairs had a minimum of 80% adhesive failures.

CONCLUSIONS

Regardless of the abutment material, additively manufactured specimens had higher bond strength and one of the subtractively manufactured materials (SM_GC) mostly had lower bond strength. The abutment material had a small effect on the bond strength. Adhesive failures were observed most frequently.

摘要

问题陈述

已经推出了几种用于临时和最终固定牙科修复体的添加剂和减法制造的树脂基材料。然而,这些材料与不同种植体基台材料之间的粘结强度的知识有限。

目的

本体外研究的目的是评估添加剂和减法制造的树脂基材料与不同种植体基台材料的剪切粘结强度(SBS)。

材料和方法

从两种用于最终用途的树脂(Crowntec;AM_CT 和 VarseoSmile Crown Plus;AM_VS)和一种用于临时用途的树脂(FREEPRINT temp;AM_FP)中添加剂制造了 110 个圆盘状试件(Ø3×3mm),或者从一种纳米石墨烯增强聚甲基丙烯酸甲酯(G-CAM;SM_GC)和一种高冲击聚合物复合材料(breCAM.HIPC;SM_BC)中减法制造。从每组中分配 2 个试件进行扫描电子显微镜评估后,根据基台材料(CopraPeek;聚醚醚酮,PEEK 和 Dentium Superline 预制基台;钛,Ti)(n=10)将试件进行分组。所有试件均采用 50-µm 氧化铝进行气载颗粒喷砂处理。在 PEEK 上施加树脂底漆(Visio.link),在 Ti 试件上施加粘合底漆(Clearfil Ceramic Primer Plus)后,使用自粘树脂水泥(PANAVIA SA Cement Universal)进行粘结。所有试件均在蒸馏水中储存 24 小时(37°C),并使用万能试验机进行 SBS 测试。使用双向方差分析和 Tukey Honestly 显著差异检验分析 SBS 数据,而卡方检验用于评估基台-树脂对之间在失效模式方面的差异(α=.05)。

结果

材料类型和基台类型之间的相互作用以及材料类型的主要因素影响 SBS(P<.001)。SM_BC-PEEK 和 SM_GC 的 SBS 最低,其次是 SM_BC-Ti,而 AM_VS-PEEK 的 SBS 最高(P≤.001)。AM_CT-Ti 的 SBS 高于 AM_FP-PEEK(P=.026)。SM_GC 的 SBS 最低,AM_VS 的 SBS 最高,而 AM_CT 和 AM_FP 的 SBS 高于 SM_BC(P≤.004)。测试材料-基台对之间的失效模式分布明显不同,而在测试材料中仅 AM_CT 存在差异(P≤.025)。大多数材料-基台对的粘合强度至少为 80%的粘合失效。

结论

无论基台材料如何,添加剂制造的试件具有更高的粘结强度,其中一种减法制造的材料(SM_GC)的粘结强度通常较低。基台材料对粘结强度的影响较小。观察到最频繁的粘合失效。

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