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内表面处理技术对增强结合力是否会影响超透明氧化锆的颜色、透明度和表面粗糙度?

Does the internal surface treatment technique for enhanced bonding affect the color, transparency, and surface roughness of ultra-transparent zirconia?

机构信息

Department of Prosthodontic Technology, School of Medicine, Tianjin Stomatological Hospital, Nankai University, Tianjin, PR China.

Tianjin Key Laboratory of Oral and Maxillofacial Function Reconstruction, Tianjin, PR China.

出版信息

Clin Oral Investig. 2024 Aug 7;28(9):473. doi: 10.1007/s00784-024-05847-4.

Abstract

PURPOSE

To investigate the effects of different surface treatments and thicknesses on the color, transparency, and surface roughness of ultra-transparent zirconia.

METHODS

A total of 120 Katana ultra-translucent multi-layered zirconia specimens were divided into 12 groups according to the thickness (0.3, 0.5, and 0.7 mm) and surface treatment (control, airborne particle abrasion [APA], lithium disilicate coating, and glaze on). Color difference (ΔE) and relative translucency parameter (RTP) were calculated using a digital spectrophotometer. The surface roughness (Ra, Rq, Sa, and Sq) was measured using a non-contact profile scanner. The surface morphologies and microstructures of the samples were observed using a tungsten filament scanning electron microscope. Statistical analyses were performed by one-way and two-way analysis of variance (ANOVA) followed by post hoc multiple comparisons and Pearson's correlation (α = 0.05).

RESULTS

The results showed that the surface treatment, ceramic thickness, and their interactions had significant effects on ΔE and RTP (p < 0.001). The surface treatment significantly altered the micromorphology and increased the surface roughness of the ceramic samples. APA exhibited the lowest transparency, largest color difference, and highest surface roughness. Zirconia with 0.3 mm and 0.7 mm thicknesses showed strong negative correlations between Sa and RTP.

CONCLUSIONS

The three internal surface treatments significantly altered the surface roughness, color difference, and transparency of ultra-transparent zirconia. As the thickness increased, the influence of the inner surface treatment on the color difference and transparency of zirconia decreased.

CLINICAL IMPLICATIONS

For new zirconia internal surface treatment technologies, in addition to considering the enhancement effect on the bonding properties, the potential effects on the color and translucency of high-transparency zirconia should also be considered. Appropriately increasing the thickness of zirconia restorations helps minimize the effect of surface treatment on the optical properties.

摘要

目的

研究不同表面处理和厚度对超透氧化锆颜色、透明度和表面粗糙度的影响。

方法

将 120 个 Katana 超透多层氧化锆试件按厚度(0.3、0.5 和 0.7mm)和表面处理(对照、喷丸处理、硅酸锂涂层和上釉)分为 12 组。使用数字分光光度计计算颜色差异(ΔE)和相对透光率参数(RTP)。使用非接触式轮廓扫描仪测量表面粗糙度(Ra、Rq、Sa 和 Sq)。使用钨灯丝扫描电子显微镜观察样品的表面形貌和微观结构。采用单因素和双因素方差分析(ANOVA)进行统计分析,随后进行多重比较和 Pearson 相关分析(α=0.05)。

结果

结果表明,表面处理、陶瓷厚度及其相互作用对 ΔE 和 RTP 有显著影响(p<0.001)。表面处理显著改变了陶瓷样品的微观形貌并增加了表面粗糙度。喷丸处理显示出最低的透明度、最大的颜色差异和最高的表面粗糙度。厚度为 0.3mm 和 0.7mm 的氧化锆之间 Sa 与 RTP 呈强烈负相关。

结论

三种内部表面处理显著改变了超透氧化锆的表面粗糙度、颜色差异和透明度。随着厚度的增加,内表面处理对氧化锆颜色差异和透明度的影响减小。

临床意义

对于新的氧化锆内表面处理技术,除了考虑对粘结性能的增强效果外,还应考虑其对高透明度氧化锆颜色和透明度的潜在影响。适当增加氧化锆修复体的厚度有助于最大限度地减少表面处理对光学性能的影响。

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