Ukkunda Neeta S, Santhoshkumar P, Paranthaman R, Moses J A
Computational Modeling and Nanoscale Processing Unit, National Institute of Food Technology Entrepreneurship and Management - Thanjavur (NIFTEM-T), Ministry of Food Processing Industries, Government of India, Thanjavur, Tamil Nadu, India.
Crit Rev Food Sci Nutr. 2025;65(24):4660-4675. doi: 10.1080/10408398.2024.2395487. Epub 2024 Aug 27.
X-ray diffraction (XRD) is an analytical technique that has found several applications focusing on the identification of crystal structure, space groups, plane, and orientation, in addition to qualitative and quantitative phase identification, and polymorphism behavior. An XRD diffractogram pattern/Bragg's peak can also provide valuable information that can be used for various food applications. While this review details the fundamental principles of XRD, the types of XRD systems, instrumentation, and the components thereof, the focus is to serve as a structured resource on explored applications of XRD in food, majorly revolving around food quality and safety. While recent studies relevant to the field are highlighted, leads for futuristic prospects are presented. With its unique approach, the XRD analysis can prove to be a rapid, robust, and sensitive nondestructive approach to food quality evaluation. Recent reports indicate its scope for nonconventional applications such as the assessment of 3D printability of foods, ice crystal formation, and screening food adulterants. Studies also highlight its scope to complement or replace conventional food quality testing approaches that involve the usage of chemicals, extensive sample preparation procedures, derivatization steps and demand long testing times.
X射线衍射(XRD)是一种分析技术,除了用于定性和定量相鉴定以及多晶型行为分析外,还在晶体结构、空间群、平面和取向的识别方面有多种应用。XRD衍射图谱/布拉格峰还能提供有价值的信息,可用于各种食品应用。虽然本综述详细介绍了XRD的基本原理、XRD系统的类型、仪器及其组件,但重点是作为一份关于XRD在食品中应用的结构化资源,主要围绕食品质量和安全展开。文中突出了该领域的近期相关研究,并展示了未来前景的线索。凭借其独特的方法,XRD分析可被证明是一种快速、可靠且灵敏的食品质量评估无损方法。近期报告表明其在非常规应用方面的潜力,如食品3D打印性评估、冰晶形成以及食品掺假物筛查。研究还强调了其补充或替代传统食品质量检测方法的潜力,传统方法涉及使用化学物质、繁琐的样品制备程序、衍生化步骤且需要较长检测时间。