Gammer Christoph, Issa Inas, Minor Andrew M, Ritchie Robert O, Kiener Daniel
Erich Schmid Institute of Materials Science, Austrian Academy of Sciences, Jahnstrasse 12, Leoben, A-8700, Austria.
Department Materials Science, Chair of Materials Physics, Montanuniversität Leoben, Jahnstrasse 12, Leoben, A-8700, Austria.
Small Methods. 2024 Dec;8(12):e2400654. doi: 10.1002/smtd.202400654. Epub 2024 Sep 6.
Understanding material failure on a fundamental level is a key aspect in the design of robust structural materials, especially for metals and alloys capable to undergo plastic deformation. In the last decade, significant progress is made in quantifying the stresses associated with failure in both experiments and simulations. Nonetheless, the processes occurring on the most essential level of individual dislocations that govern semi-brittle and ductile fracture are still experimentally not accessible, limiting the failure prediction capabilities. Therefore, in the present work, a one-of-a-kind nanoscale fracture experiment is conducted on a single crystalline Cr bending beam in situ in the transmission electron microscope and for the first time quantify the transient strains around individual dislocations, as well as of the whole dislocation network during crack opening. The results reveal the importance of both pre-existing and newly emitted dislocations for crack-tip shielding via their intrinsic strain field and provide guidelines to design more damage tolerant materials.
从基本层面理解材料失效是设计坚固结构材料的关键方面,特别是对于能够发生塑性变形的金属和合金而言。在过去十年中,在实验和模拟中量化与失效相关的应力方面取得了重大进展。然而,在控制半脆性和延性断裂的单个位错的最基本层面上发生的过程在实验上仍然无法实现,这限制了失效预测能力。因此,在本工作中,在透射电子显微镜中原位对单晶Cr弯曲梁进行了独一无二的纳米级断裂实验,并首次量化了单个位错周围以及裂纹张开期间整个位错网络的瞬态应变。结果揭示了既有位错和新发射位错通过其固有应变场对裂纹尖端屏蔽的重要性,并为设计更具损伤容限的材料提供了指导。