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牛奶中脱氧雪腐镰刀菌烯醇的快速筛选。

Fast screening of Milk for Deoxynivalenol.

机构信息

Laboratory of Electrochemistry and PATLAB Bucharest, National Institute of Research for Electrochemistry and Condensed Matter, Bucharest 060021, Romania; National University of Science and Technology POLITEHNICA of Bucharest, Faculty of Chemical Engineering and Biotechnologies, Romania.

Laboratory of Electrochemistry and PATLAB Bucharest, National Institute of Research for Electrochemistry and Condensed Matter, Bucharest 060021, Romania; National University of Science and Technology POLITEHNICA of Bucharest, Faculty of Chemical Engineering and Biotechnologies, Romania.

出版信息

Food Chem. 2025 Jan 15;463(Pt 2):141337. doi: 10.1016/j.foodchem.2024.141337. Epub 2024 Sep 16.

DOI:10.1016/j.foodchem.2024.141337
PMID:39298844
Abstract

A 2D platform was designed and validated for fast screening of milk for deoxynivalenol. The qualitative and quantitative assay of deoxynivalenol in the milk samples was done using a 2D stochastic sensor based on single walled carbon nanotubes modified with [N-(pyridine-4-yl-methyl)]octadec-9-enamide. The working concentration range was between 10 and 10 g mL, with a sensitivity of 5.48 × 10 sgmL, and a limit of determination of 1 fg mL. Recovery values higher than 99.00 % with RSD values lower than 1.00 % were recorded for the determination of deoxynivalenol in cow's and in the vegetarian (coconut milk, soy milk, almond milk) milk.

摘要

设计并验证了一个二维平台,用于快速筛选牛奶中的脱氧雪腐镰刀菌烯醇。使用基于单壁碳纳米管的二维随机传感器,对牛奶样品中的脱氧雪腐镰刀菌烯醇进行定性和定量分析,该传感器用[N-(吡啶-4-基-甲基)]十八-9-烯酰胺修饰。工作浓度范围为 10 至 10 g/mL,灵敏度为 5.48×10 sg/mL,检测限为 1 fg/mL。在牛奶(奶牛和素食者的,如椰奶、豆浆、杏仁奶)中测定脱氧雪腐镰刀菌烯醇时,回收率高于 99.00%,相对标准偏差(RSD)低于 1.00%。

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