Hu Chao, Chen Jiankui, Chen Wei, Tang Wei, Wang Guozhen, Pan Fei, Yin Zhouping
State Key Laboratory of Intelligent Manufacturing Equipment and Technology, School of Mechanical Science and Engineering, Huazhong University of Science and Technology, Wuhan 430074, PR China.
Wuhan National Innovation Technology Optoelectronics Equipment Co., Ltd, Wuhan 430074, PR China.
ACS Omega. 2024 Sep 6;9(37):38970-38988. doi: 10.1021/acsomega.4c05402. eCollection 2024 Sep 17.
Electrohydrodynamic atomization coating technology is well-suited for micro-/nanoscale thin-film additive manufacturing. However, there are still some challenges in quality control and parameter adjustment during the coating process. Especially when coating on nonconductive and nonhydrophilic substrates, film quality and thickness uniformity are difficult to control. This paper proposes an optimization strategy for enhancing the efficiency and quality of thin-film manufacturing on nonconductive, nonhydrophilic glass substrates. In this paper, a visual inspection system was developed for in situ inspection and identification of droplet deposition states in the substrate surface. Then, the statistical relationship between the operating parameters and the quality of the deposition state was analyzed by response surface methodology. On this basis, machine learning models and intelligent recommendation frameworks for small data sets were developed to rapidly optimize operating parameters and improve the quality of thin-film coating. Optimization strategy developed by applying the principles of statistical modeling, analysis of variance, and global optimization are more efficient and less costly than traditional parameter screening methods. The experimental results show that optimum deposition quality can be obtained with the recommended operating parameters. And, validation results show a 12.8% improvement in film thickness uniformity. At the same time, no mura defects appeared on the thin-film surface. The proposed optimization strategy can improve the efficiency and quality of additive manufacturing of micro and nano thin films and is beneficial for advancing industrial applications of the electrohydrodynamic atomization coating.
电流体动力学雾化涂层技术非常适合微纳尺度的薄膜增材制造。然而,在涂层过程中的质量控制和参数调整方面仍然存在一些挑战。特别是在非导电和非亲水性基材上进行涂层时,薄膜质量和厚度均匀性难以控制。本文提出了一种优化策略,以提高在非导电、非亲水性玻璃基材上制造薄膜的效率和质量。本文开发了一种视觉检测系统,用于原位检测和识别基材表面的液滴沉积状态。然后,通过响应面法分析操作参数与沉积状态质量之间的统计关系。在此基础上,开发了针对小数据集的机器学习模型和智能推荐框架,以快速优化操作参数并提高薄膜涂层质量。应用统计建模、方差分析和全局优化原理开发的优化策略比传统的参数筛选方法更高效、成本更低。实验结果表明,使用推荐的操作参数可以获得最佳的沉积质量。而且,验证结果表明薄膜厚度均匀性提高了12.8%。同时,薄膜表面未出现条纹缺陷。所提出的优化策略可以提高微纳薄膜增材制造的效率和质量,有利于推动电流体动力学雾化涂层的工业应用。