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使用1064纳米调Q纳秒脉冲激光和环己烷快速制备超疏水Ti-6Al-4V表面

Fast fabrication of superhydrophobic Ti-6Al-4V surface using Q-switched nanosecond pulsed laser at 1064 nm and cyclohexane.

作者信息

Haryono Muhammad Budi, Lin Kaung Wai Yan, Waritanant Tanant

机构信息

School of Materials Science and Innovation, Faculty of Science, Mahidol University, Thailand.

出版信息

Heliyon. 2024 Sep 11;10(18):e37808. doi: 10.1016/j.heliyon.2024.e37808. eCollection 2024 Sep 30.

DOI:10.1016/j.heliyon.2024.e37808
PMID:39315134
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11417309/
Abstract

Superhydrophobic and superhydrophilic surfaces are attracting significant attention in fundamental and applied research. This study fabricated the micro/nanostructure with a Q-switched nanosecond pulsed laser on the Ti-6Al-4V surface. Three laser-generated surface topographies on titanium were produced based on three different pitch sizes (51 μm, 34 μm, and 29 μm). The laser textured surfaces (LTS) were studied in terms of both structure evolution and chemical composition using Field Emission Scanning Electron Microscopy (FE-SEM), Optical Microscopy (OM), Confocal Laser Scanning Microscopy (CLSM), Raman Spectroscopy, and X-ray Diffractometer (XRD). 29 μm pitch displayed the lowest water contact angle of 18.5° and surface roughness of 0.5 μm. This structure was further treated with cyclohexane at different temperatures. The best sample reached superhydrophobicity with a maximum water contact angle of 155.1° immediately after being treated with cyclohexane at the low temperature of 70 °C for 2 h, while the raw surface, for comparison, showed no change in hydrophobicity after being treated with cyclohexane under the same condition. Thus showing clear evidence of a combined effect between LTS and post-treatment. The surface features were assessed to explain the underlying process.

摘要

超疏水和超亲水表面在基础研究和应用研究中都备受关注。本研究利用调Q纳秒脉冲激光在Ti-6Al-4V表面制备了微/纳米结构。基于三种不同的间距尺寸（51μm、34μm和29μm）在钛表面产生了三种激光生成的表面形貌。使用场发射扫描电子显微镜（FE-SEM）、光学显微镜（OM）、共聚焦激光扫描显微镜（CLSM）、拉曼光谱和X射线衍射仪（XRD）对激光织构表面（LTS）的结构演变和化学成分进行了研究。29μm间距的表面显示出最低的水接触角，为18.5°，表面粗糙度为0.5μm。对该结构在不同温度下用环己烷进一步处理。最佳样品在70°C低温下用环己烷处理2小时后，立即达到超疏水性，最大水接触角为155.1°，而作为对比的原始表面在相同条件下用环己烷处理后疏水性没有变化。从而清楚地证明了激光织构表面和后处理之间的联合作用。对表面特征进行了评估以解释其潜在过程。

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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/2cb350081690/ga1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/622edf44341a/gr1.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/a0fe7119fcd7/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/4f2ad6254f2a/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/dcc97d920680/gr6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/da821ee51d11/gr7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/911a58bb8fbd/gr8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/01ced524b987/gr9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/60aa32222cda/gr10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/431d2eaacf13/gr11.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/c7796eaace23/gr12.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/af74ff46cf7c/gr13.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/9b3472b4bec2/gr14.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/32a95539d5dd/gr15.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/b47aa8e6fc9c/gr16.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/868555b73655/gr17.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/96eaebfb940b/gr18.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d01f/11417309/882adadb58d2/gr19.jpg

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