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“茶枝柑”幼果黄酮提取物的微胶囊制备及其性质

Microcapsule Preparation and Properties of Flavonoid Extract from Immature 'Chachiensis' Peel.

作者信息

Zhang Xinyi, Li Qili, Wu Sisi, Liu Yan, Chen Jiaxu, Li Tao, Su Donglin

机构信息

Longping Branch, Graduate School of Hunan University, Changsha 410125, China.

Hunan Agricultural Product Processing Institute, Hunan Academy of Agricultural Sciences, Changsha 410125, China.

出版信息

Foods. 2024 Sep 27;13(19):3096. doi: 10.3390/foods13193096.

Abstract

'Chachiensis' is a citrus cultivar in the Rutaceae family, and its peel is commonly utilized as a raw material for Guangchenpi. This study used flavonoid extract from the peel of immature 'Chachiensis' (CCE) as the raw material to investigate the encapsulation ability of different wall materials (plant-based proteins, including soybean protein isolation (SPI), pea protein (PP), and zein; carbohydrates, including maltodextrin (MD), Momordica charantia polysaccharide (MCP), and gum acacia (GA); and composite wall materials of both types) on CCE. The wall material with the highest encapsulation rate was selected for the preparation of CCE microcapsules. Furthermore, the physicochemical characteristics, antioxidant capacity, bioavailability, and storage stability of the CCE microcapsules were explored. The results indicated that among all wall materials, the composite wall material PPMD had the highest encapsulation rate, which was 84.44 ± 0.34%. After encapsulation, the microcapsules tended to have a yellow color and exhibited characteristics such as system stability, low moisture content, and low hygroscopicity. In vitro antioxidant assays revealed that the encapsulation of CCE significantly increased the scavenging rates of DPPH and ABTS free radicals. In vitro gastrointestinal digestion experiments indicated that the release rate of PPMD-CCE in intestinal fluid was significantly greater than that of free CCE, ultimately reaching 85.89 ± 1.53%. Storage experiments demonstrated that after 45 days under various temperature and light conditions, the retention rate of CCE in the microcapsules was significantly greater than that of free CCE. The above findings provide new possibilities for the application of PP and plant proteins and lay a foundation for the future industrial application of CCE.

摘要

“茶枝柑”是芸香科柑橘属的一个栽培品种,其果皮通常被用作广陈皮的原料。本研究以未成熟“茶枝柑”果皮中的黄酮提取物(CCE)为原料,研究了不同壁材(植物蛋白,包括大豆分离蛋白(SPI)、豌豆蛋白(PP)和玉米醇溶蛋白;碳水化合物,包括麦芽糊精(MD)、苦瓜多糖(MCP)和阿拉伯胶(GA);以及两者的复合壁材)对CCE的包封能力。选择包封率最高的壁材来制备CCE微胶囊。此外,还探究了CCE微胶囊的理化特性、抗氧化能力、生物利用度和储存稳定性。结果表明,在所有壁材中,复合壁材PPMD的包封率最高,为84.44±0.34%。包封后,微胶囊呈黄色,具有体系稳定性、低水分含量和低吸湿性等特点。体外抗氧化试验表明,CCE的包封显著提高了DPPH和ABTS自由基的清除率。体外胃肠消化实验表明,PPMD-CCE在肠液中的释放率显著高于游离CCE,最终达到85.89±1.53%。储存实验表明,在不同温度和光照条件下放置45天后,微胶囊中CCE的保留率显著高于游离CCE。上述研究结果为PP和植物蛋白的应用提供了新的可能性,为CCE的未来工业化应用奠定了基础。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/116b/11475909/4c2d6695596a/foods-13-03096-g001.jpg

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