Chen Jian, Jin Xinyuan, Geng Jiwei, Luo Xianhui, Li Yugang, Xia Peikang, Li Xianfeng, Wang Fangming, Chen Dong, Wang Mingliang, Wang Haowei
State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, No. 800 Dongchuan Road, Shanghai 200240, China.
State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, No. 800 Dongchuan Road, Shanghai 200240, China.
Ultrason Sonochem. 2024 Dec;111:107092. doi: 10.1016/j.ultsonch.2024.107092. Epub 2024 Oct 15.
Hydrogen removal from particle-reinforced Al composite is critical for preventing porosities near particle clusters and improving comprehensive material properties. This study investigated the effects of different argon flow schemes and power ultrasound on bubble dispersion in water. Based on similarity theory, the optimal argon flow scheme for ultrasonic-assisted argon (UAA) treatment was identified and applied to TiB/2024 Al composite to explore the degassing mechanism. Three argon flow schemes for UAA treatment: EV-EC (External ventilation, equal channel), IV-EC (Internal ventilation, equal channel), and IV-RC (Internal ventilation, reduced channel) were evaluated through numerical simulation and water simulation experiments. The results demonstrated that IV-RC scheme exhibits superior bubble dispersion characteristics and a broader bubbling range. Experimental results in Al composite confirmed that UAA treatment with IV-RC scheme achieved the highest degassing efficiency, with a relative density improvement of up to 98.01 % and the lowest hydrogen content (0.0235 ppm). Synchrotron radiation X-ray computed tomography results indicated that UAA treatment effectively reduces the pore size and volume, transforming interconnected, complex pores into dispersed, nearly spherical ones. Ultrasonic cavitation aids this process by breaking small argon bubbles into numerous tiny bubbles that penetrate deeply into the melt, reducing the wettability angle between particles and the matrix and thereby improving hydrogen removal efficiency.
从颗粒增强铝基复合材料中去除氢气对于防止颗粒簇附近出现孔隙以及改善材料综合性能至关重要。本研究调查了不同氩气流动方案和功率超声对水中气泡分散的影响。基于相似理论,确定了超声辅助氩气(UAA)处理的最佳氩气流动方案,并将其应用于TiB/2024铝基复合材料以探究除气机制。通过数值模拟和水模拟实验评估了UAA处理的三种氩气流动方案:EV-EC(外部通气,等通道)、IV-EC(内部通气,等通道)和IV-RC(内部通气,变通道)。结果表明,IV-RC方案具有卓越的气泡分散特性和更宽的鼓泡范围。铝基复合材料的实验结果证实,采用IV-RC方案的UAA处理实现了最高的除气效率,相对密度提高高达98.01%,氢含量最低(0.0235 ppm)。同步辐射X射线计算机断层扫描结果表明,UAA处理有效减小了孔径和孔隙体积,将相互连通的复杂孔隙转变为分散的近球形孔隙。超声空化通过将小氩气泡破碎成众多微小气泡并使其深入渗透到熔体中,降低颗粒与基体之间的润湿性角度,从而提高了氢去除效率。