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优化泡沫垫干燥工艺以制备高品质番茄粉:响应面法研究

Optimization of the foam-mat drying process to develop high-quality tomato powder: A response surface methodology approach.

作者信息

Hossain Mohammad Afzal, Ahmed Tanvir, Ferdaus Jannatul, Zzaman Wahidu

机构信息

Department of Food Engineering and Tea Technology, Shahjalal University of Science and Technology, Sylhet, 3114, Bangladesh.

出版信息

Heliyon. 2024 Oct 24;10(21):e39811. doi: 10.1016/j.heliyon.2024.e39811. eCollection 2024 Nov 15.

Abstract

This research aimed to estimate the optimum formulation of process parameters in making tomato powder with optimal physicochemical properties using foam-mat drying. The egg albumin (EA) concentration (1-5%), carboxymethyl cellulose (CMC) concentration (1-1.5 %), and drying temperature (60-70 °C) were employed as independent variables in optimizing through Response Surface Methodology (RSM) in combination with Box-Behnken experimental design (BBD). Based on the total 17 runs of BBD, foam-mat dried powder showed physicochemical properties such as 0.18-0.33 g/cm foam density, 178.54-350 % foam expansion, 40-94 % foam stability, 46.80-62 % water soluble index (WSI), 1.13-2.96 water absorption index (WAI), 1.51-2 °Brix TSS, 2.30-3.98 mg/100 mL ascorbic acid, 0.22-0.38 % titratable acidity, and color (L∗: 29.26-48.07, a∗: 9.73-16.86, and b∗: 6.81-21.56). Furthermore, the ANOVA findings revealed the correlation of determination (R) exceeding 85 % for the models, suggesting that the interaction between the responses and the prediction of the implied model is suitable. The optimal formulation from RSM was 4.59 % EA, 0.70 % CMC, and 60 °C drying temperature. Under the optimized conditions, the experimental values were 0.19 ± 0.03 g/cm foam density, 346.60 ± 3.35 % foam expansion, 89.05 ± 2.80 % foam stability, 55.56 ± 3.22 % WSI, 2.49 ± 0.09 WAI, 1.84 ± 0.15 °Brix TSS, 2.93 ± 0.10 mg/100 mL ascorbic acid, 0.39 ± 0.02 % titratable acidity, 46.95 ± 6.35 L∗, 17.54 ± 1.50 a∗, and 21.85 ± 0.74 b∗. The optimized parameters were verified, and there was good agreement between the experimental results and the predicted values (residual standard error (RSE) ≤ 5).

摘要

本研究旨在通过泡沫垫干燥法,估算制备具有最佳物理化学性质的番茄粉时工艺参数的最佳配方。蛋清蛋白(EA)浓度(1 - 5%)、羧甲基纤维素(CMC)浓度(1 - 1.5%)和干燥温度(60 - 70°C)作为自变量,通过响应面法(RSM)结合Box - Behnken实验设计(BBD)进行优化。基于BBD的总共17次运行,泡沫垫干燥粉末呈现出如下物理化学性质:泡沫密度为0.18 - 0.33 g/cm,泡沫膨胀率为178.54 - 350%,泡沫稳定性为40 - 94%,水溶性指数(WSI)为46.80 - 62%,吸水性指数(WAI)为1.13 - 2.96,总可溶性固形物(TSS)为1.51 - 2°Brix,抗坏血酸含量为2.30 - 3.98 mg/100 mL,可滴定酸度为0.22 - 0.38%,颜色(L∗:29.26 - 48.07,a∗:9.73 - 16.86,b∗:6.81 - 21.56)。此外,方差分析结果显示,模型的决定系数(R)超过85%,这表明响应与隐含模型预测之间的相互作用是合适的。RSM得出的最佳配方为4.59%的EA、0.70%的CMC和60°C的干燥温度。在优化条件下,实验值为:泡沫密度0.19±0.03 g/cm,泡沫膨胀率346.60±3.35%,泡沫稳定性89.05±2.80%,WSI为55.56±3.22%,WAI为2.49±0.09,TSS为1.84±0.15°Brix,抗坏血酸含量为2.93±0.10 mg/100 mL,可滴定酸度为0.39±0.02%,颜色L∗为46.95±6.35,a∗为17.54±1.50,b∗为21.85±0.74。对优化后的参数进行了验证,实验结果与预测值之间具有良好的一致性(残差标准误差(RSE)≤5)。

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