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一种能够在软X射线能量下进行电子产额检测的全封闭式样品架。

A fully contained sample holder capable of electron-yield detection at soft X-ray energies.

作者信息

Gunther S Olivia, Smith Patrick W, Branson Jacob A, Ditter Alexander S, Minasian Stefan G, N'Diaye Alpha T, Schacherl Bianca, Shuh David K

机构信息

Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA.

出版信息

J Synchrotron Radiat. 2025 Jan 1;32(Pt 1):230-233. doi: 10.1107/S1600577524011354.

DOI:10.1107/S1600577524011354
PMID:39705250
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11708856/
Abstract

A holder has been developed that enables electron yield-detected soft X-ray spectroscopy of fully contained samples at low temperature. Crucially, this design uses elements of the sample containment to collect ejected electrons, removing the need to expose samples directly to the vacuum environment of the spectrometer. The design is modular and should be adaptable to a number of different endstation configurations, enabling spectroscopy of air-sensitive, radioactive and vacuum-sensitive (biological) samples.

摘要

已经开发出一种支架,能够在低温下对完全封闭的样品进行电子产额检测软X射线光谱分析。至关重要的是,这种设计利用样品容器的部件来收集出射电子,从而无需将样品直接暴露于光谱仪的真空环境中。该设计是模块化的,应该能够适应多种不同的终端站配置,从而实现对空气敏感、放射性和真空敏感(生物)样品的光谱分析。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4e77/11708856/0f9521ea05de/s-32-00230-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4e77/11708856/5c8c0e8debf2/s-32-00230-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4e77/11708856/0f9521ea05de/s-32-00230-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4e77/11708856/5c8c0e8debf2/s-32-00230-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4e77/11708856/0f9521ea05de/s-32-00230-fig2.jpg

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