de Sousa Silva Nayara, Silva Gezaildo Santos, Grisi Cristiani Viegas Brandão, Vieira Vanessa Bordin, Dantas Carlos Eduardo Alves, Guimarães George Henrique Camêlo, Maciel Maria Inês Sucupira
Graduate Program in Food Science and Technology, Federal University of Paraíba, 58051-900 João Pessoa, Paraíba, Brazil.
Graduate Program in Chemical Engineering, Federal University of Paraíba, Center for Human, Social, and Agricultural Sciences, 58051-900 João Pessoa, Paraíba, Brazil.
Int J Biol Macromol. 2025 Apr;298:139546. doi: 10.1016/j.ijbiomac.2025.139546. Epub 2025 Jan 12.
This study aimed to investigate the impact of adding aroeira leaf extract (Schinus terebinthifolius Raddi) to a yam starch film matrix, focusing on the development of potentially active films and the evaluation of their physicochemical, mechanical, optical, and antioxidant properties. Films were produced using the casting method with varying extract concentrations (0, 3, 6, 12, and 15 %), yam starch (2 %), and glycerol (1 %). The antioxidant properties were analyzed by determining the total phenolic content, 2,2-Diphenyl-1-Picrylhydrazyl (DPPH) radical scavenging, ferric reducing power, and 2,2-azinobis (3-ethylbenzothiazoline-6-sulfonic acid) (ABTS) radical elimination, which revealed a significant increase in antioxidant properties as the extract concentration increased. The incorporation of the extract resulted in increased film thickness and decreased solubility, water activity, and moisture, as well as changes in brightness (L*), tensile strength, and elongation. X-ray diffraction (XRD) showed an increase in the crystallinity of the films, whereas Fourier-transform infrared (FTIR) analysis revealed similar spectra among the films. The thermal stability did not exhibit significant variations with the addition of the extract, indicating high heat resistance. Films with 15 % extract showed changes in the surface microstructure, indicating greater roughness than the control film. Thus, formulations with 3 %, 6 %, and 9 % aroeira extract emerged as the most promising, suggesting their potential for application in active packaging and as a sustainable alternative for food preservation.
本研究旨在探讨在山药淀粉膜基质中添加巴西胡椒叶提取物(Schinus terebinthifolius Raddi)的影响,重点是开发具有潜在活性的薄膜,并评估其物理化学、机械、光学和抗氧化性能。采用流延法制备薄膜,其中提取物浓度(0%、3%、6%、12%和15%)、山药淀粉(2%)和甘油(1%)各不相同。通过测定总酚含量、2,2-二苯基-1-苦基肼(DPPH)自由基清除能力、铁还原能力和2,2-联氮-双-(3-乙基苯并噻唑啉-6-磺酸)(ABTS)自由基清除能力来分析抗氧化性能,结果表明随着提取物浓度的增加,抗氧化性能显著提高。提取物的加入导致薄膜厚度增加,溶解度、水分活度和水分降低,同时亮度(L*)、拉伸强度和伸长率也发生了变化。X射线衍射(XRD)显示薄膜的结晶度增加,而傅里叶变换红外光谱(FTIR)分析表明各薄膜的光谱相似。添加提取物后热稳定性没有显著变化,表明具有高耐热性。含有15%提取物的薄膜表面微观结构发生了变化,表明比对照薄膜更粗糙。因此,含有3%、6%和9%巴西胡椒提取物的配方表现出最大的潜力,表明它们在活性包装中的应用潜力以及作为食品保鲜的可持续替代品的潜力。