García Arantzazu Valdés, Álvarez-Pérez Olga B, Rojas Romeo, Aguilar Cristobal N, Garrigós María Carmen
Analytical Chemistry, Nutrition & Food Sciences Department, University of Alicante, P.O. Box 99, 03080 Alicante, Spain.
Food Research Department, School of Chemistry, Universidad Autónoma de Coahuila, Saltillo 25280, Coahuila, Mexico.
Foods. 2020 Sep 22;9(9):1339. doi: 10.3390/foods9091339.
Active edible films based on corn starch containing glycerol as a plasticizer and an olive extract obtained from Spanish olive fruit () by-products (olive extract; OE) at different concentrations (0, 0.05, 0.1 and 0.2 wt%) were prepared by using the casting technique and further solvent-evaporation. OE showed high total phenolic and flavonoids contents and antioxidant activity, which was evaluated by using three different methods: free radical scavenging assay by (1, 1-Dipheny l-2-picrylhydrazyl) DPPH, 2, 2-Azino-bis (3-ethylbenzothiazoline-6-sulfonic acid) ABTS radical inhibition and ferric reducing antioxidant power (FRAP). The incorporation of OE into the corn starch/glycerol matrix underlined the antioxidant potential and antimicrobial effect against and of these novel active films, being noticeable for films added with 0.2 wt% OE. The developed active films showed a clear thermo-oxidative stability improvement with OE incorporation, in particular at 0.2 wt% loading with an increase of around 50 °C in the initial degradation temperature (T) and oxidation onset temperature (OOT). The functional properties of control films were also improved with OE addition resulting in a decrease in Young's modulus, elongation at break, shore D hardness and water vapor permeability. The present work suggested the potential of the developed corn starch-based edible films as low-price and sustainable food packaging systems to prevent the oxidative deterioration of packaged foodstuff while reducing also the generation of olive by-products.
基于玉米淀粉制备了活性可食性薄膜,该薄膜含有作为增塑剂的甘油以及从西班牙橄榄果()副产品中获得的不同浓度(0、0.05、0.1和0.2 wt%)的橄榄提取物(橄榄提取物;OE),采用流延技术并进一步通过溶剂蒸发法制备。OE显示出高总酚和黄酮含量以及抗氧化活性,通过三种不同方法对其进行评估:采用(1,1 - 二苯基 - 2 - 苦基肼)DPPH进行自由基清除测定、2,2 - 联氮 - 双(3 - 乙基苯并噻唑啉 - 6 - 磺酸)ABTS自由基抑制以及铁还原抗氧化能力(FRAP)。将OE掺入玉米淀粉/甘油基质中突出了这些新型活性薄膜的抗氧化潜力和对 和 的抗菌效果,对于添加0.2 wt% OE的薄膜尤为明显。随着OE的掺入,所制备的活性薄膜的热氧化稳定性明显提高,特别是在0.2 wt%的添加量下,初始降解温度(T)和氧化起始温度(OOT)提高了约50°C。添加OE还改善了对照薄膜的功能特性,导致杨氏模量、断裂伸长率、邵氏D硬度和水蒸气透过率降低。本研究表明,所开发的基于玉米淀粉的可食性薄膜有潜力作为低价且可持续的食品包装系统,以防止包装食品的氧化变质,同时减少橄榄副产品的产生。