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3D打印和铣削5Y部分稳定氧化锆的双轴弯曲强度和维氏硬度

Biaxial Flexural Strength and Vickers Hardness of 3D-Printed and Milled 5Y Partially Stabilized Zirconia.

作者信息

Hetzler Sebastian, Hinzen Carina, Rues Stefan, Schmitt Clemens, Rammelsberg Peter, Zenthöfer Andreas

机构信息

Department of Prosthodontics, Medical Faculty, Heidelberg University, Im Neuenheimer Feld 400, 69120 Heidelberg, Germany.

出版信息

J Funct Biomater. 2025 Jan 20;16(1):36. doi: 10.3390/jfb16010036.

Abstract

This study compares the mechanical properties of 5-mol% yttria partially stabilized zirconia (5Y-PSZ) materials, designed for 3D printing or milling. Three 5Y-PSZ materials were investigated: printed zirconia (PZ) and two milled zirconia materials, VITA-YZ-XT (MZ-1) and Cercon xt (MZ-2). PZ samples were made from a novel ceramic suspension via digital light processing and divided into three subgroups: PZ-HN-ZD (horizontal nesting, printed with Zipro-D Dental), PZ-VN-Z (vertical nesting, printed with Zipro-D Dental) and PZ-VN-Z (vertical nesting, printed with Zipro Dental). Key outcomes included biaxial flexural strength (ISO 6872) and Vickers hardness ( ≥ 23 samples/subgroup). Microstructure and grain size were analyzed using light and scanning electron microscopy. Printed specimens exhibited biaxial flexural strengths of 1059 ± 178 MPa (PZ-HN-ZD), 797 ± 135 MPa (PZ-VN-ZD), and 793 ± 75 MPa (PZ-VN-Z). Milled samples showed strengths of 745 ± 96 MPa (MZ-1) and 928 ± 87 MPa (MZ-2). Significant differences (α = 0.05) were observed, except between vertically printed groups and MZ-1. Vickers hardness was highest for PZ-VN-Z (HV0.5 = 1590 ± 24), followed by MZ-1 (HV0.5 = 1577 ± 9) and MZ-2 (HV0.5 = 1524 ± 4), with significant differences, except between PZ and MZ-1. PZ samples had the smallest grain size (0.744 ± 0.024 µm) compared to MZ-1 (0.820 ± 0.042 µm) and MZ-2 (1.023 ± 0.081 µm). All materials met ISO 6872 standards for crowns and three-unit prostheses in posterior regions.

摘要

本研究比较了设计用于3D打印或铣削的5摩尔%氧化钇部分稳定氧化锆(5Y-PSZ)材料的力学性能。研究了三种5Y-PSZ材料:打印氧化锆(PZ)以及两种铣削氧化锆材料,维他YZ-XT(MZ-1)和泽康xt(MZ-2)。PZ样品由一种新型陶瓷悬浮液通过数字光处理制成,并分为三个亚组:PZ-HN-ZD(水平嵌套,使用Zipro-D Dental打印)、PZ-VN-Z(垂直嵌套,使用Zipro-D Dental打印)和PZ-VN-Z(垂直嵌套,使用Zipro Dental打印)。关键结果包括双轴弯曲强度(ISO 6872)和维氏硬度(每个亚组≥23个样品)。使用光学显微镜和扫描电子显微镜分析微观结构和晶粒尺寸。打印试样的双轴弯曲强度分别为1059±178兆帕(PZ-HN-ZD)、797±135兆帕(PZ-VN-ZD)和793±75兆帕(PZ-VN-Z)。铣削样品的强度分别为745±96兆帕(MZ-1)和928±87兆帕(MZ-2)。观察到显著差异(α=0.05),垂直打印组和MZ-1之间除外。PZ-VN-Z的维氏硬度最高(HV0.5 = 1590±24),其次是MZ-1(HV0.5 = 1577±9)和MZ-2(HV0.5 = 1524±4),PZ和MZ-1之间除外,存在显著差异。与MZ-1(0.820±0.042微米)和MZ-2(1.023±0.081微米)相比,PZ样品的晶粒尺寸最小(0.744±0.024微米)。所有材料均符合ISO 6872标准中后牙区牙冠和三单位修复体的要求。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dab0/11766354/7528ea77edf1/jfb-16-00036-g001.jpg

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