Hetzler Sebastian, Hinzen Carina, Rues Stefan, Schmitt Clemens, Rammelsberg Peter, Zenthöfer Andreas
Department of Prosthodontics, Medical Faculty, Heidelberg University, Im Neuenheimer Feld 400, 69120 Heidelberg, Germany.
J Funct Biomater. 2025 Jan 20;16(1):36. doi: 10.3390/jfb16010036.
This study compares the mechanical properties of 5-mol% yttria partially stabilized zirconia (5Y-PSZ) materials, designed for 3D printing or milling. Three 5Y-PSZ materials were investigated: printed zirconia (PZ) and two milled zirconia materials, VITA-YZ-XT (MZ-1) and Cercon xt (MZ-2). PZ samples were made from a novel ceramic suspension via digital light processing and divided into three subgroups: PZ-HN-ZD (horizontal nesting, printed with Zipro-D Dental), PZ-VN-Z (vertical nesting, printed with Zipro-D Dental) and PZ-VN-Z (vertical nesting, printed with Zipro Dental). Key outcomes included biaxial flexural strength (ISO 6872) and Vickers hardness ( ≥ 23 samples/subgroup). Microstructure and grain size were analyzed using light and scanning electron microscopy. Printed specimens exhibited biaxial flexural strengths of 1059 ± 178 MPa (PZ-HN-ZD), 797 ± 135 MPa (PZ-VN-ZD), and 793 ± 75 MPa (PZ-VN-Z). Milled samples showed strengths of 745 ± 96 MPa (MZ-1) and 928 ± 87 MPa (MZ-2). Significant differences (α = 0.05) were observed, except between vertically printed groups and MZ-1. Vickers hardness was highest for PZ-VN-Z (HV0.5 = 1590 ± 24), followed by MZ-1 (HV0.5 = 1577 ± 9) and MZ-2 (HV0.5 = 1524 ± 4), with significant differences, except between PZ and MZ-1. PZ samples had the smallest grain size (0.744 ± 0.024 µm) compared to MZ-1 (0.820 ± 0.042 µm) and MZ-2 (1.023 ± 0.081 µm). All materials met ISO 6872 standards for crowns and three-unit prostheses in posterior regions.
本研究比较了设计用于3D打印或铣削的5摩尔%氧化钇部分稳定氧化锆(5Y-PSZ)材料的力学性能。研究了三种5Y-PSZ材料:打印氧化锆(PZ)以及两种铣削氧化锆材料,维他YZ-XT(MZ-1)和泽康xt(MZ-2)。PZ样品由一种新型陶瓷悬浮液通过数字光处理制成,并分为三个亚组:PZ-HN-ZD(水平嵌套,使用Zipro-D Dental打印)、PZ-VN-Z(垂直嵌套,使用Zipro-D Dental打印)和PZ-VN-Z(垂直嵌套,使用Zipro Dental打印)。关键结果包括双轴弯曲强度(ISO 6872)和维氏硬度(每个亚组≥23个样品)。使用光学显微镜和扫描电子显微镜分析微观结构和晶粒尺寸。打印试样的双轴弯曲强度分别为1059±178兆帕(PZ-HN-ZD)、797±135兆帕(PZ-VN-ZD)和793±75兆帕(PZ-VN-Z)。铣削样品的强度分别为745±96兆帕(MZ-1)和928±87兆帕(MZ-2)。观察到显著差异(α=0.05),垂直打印组和MZ-1之间除外。PZ-VN-Z的维氏硬度最高(HV0.5 = 1590±24),其次是MZ-1(HV0.5 = 1577±9)和MZ-2(HV0.5 = 1524±4),PZ和MZ-1之间除外,存在显著差异。与MZ-1(0.820±0.042微米)和MZ-2(1.023±0.081微米)相比,PZ样品的晶粒尺寸最小(0.744±0.024微米)。所有材料均符合ISO 6872标准中后牙区牙冠和三单位修复体的要求。