Olmos Luis, González-Pedraza Ana Silvia, Vergara-Hernández Héctor Javier, Bouvard Didier, López-Cornejo Monserrat Sofía, Servín-Castañeda Rumualdo
Universidad Michoacana de San Nicolás de Hidalgo, INICIT, Fco. J. Mujica S/N, Morelia 58060, Michoacán, Mexico.
División de Estudios de Posgrado e Investigación, Tecnológico Nacional de México/I.T. Morelia, Av. Tecnológico #1500, Colonia Lomas de Santiaguito, Morelia 58120, Michoacán, Mexico.
Materials (Basel). 2025 Jan 16;18(2):389. doi: 10.3390/ma18020389.
Nowadays, metallic bone replacement is in high demand due to different issues, like sicknesses and accidents. Thus, bone implants are fabricated with tailored properties and microstructure for long-term use in the human body. To improve such implants, 3D printing is the most promising technique. Therefore, this work aims to evaluate the fabrication of porous materials by extrusion 3D printing of Ti6Al4V. Cylindrical samples were fabricated from pellets for metal injection molding of Ti6Al4V powders, creating hexagonal channels with three different sizes. The densification kinetics was evaluated by dilatometry tests, which enabled following the densification of the samples during the sintering cycle. Subsequently, the samples were characterized by scanning electron microscopy and X-ray computed tomography to analyze their microstructure. Compression tests evaluated the mechanical strength of sintered samples. It was found that the hexagonal shape during printing is better defined as the channel size increases. The results show similar behavior for each of the channel sizes during sintering; however, greater densification is obtained as the channel size decreases. Additionally, microporosity is obtained at the particle level, which is completely interconnected, ensuring the passage of fluids through the entire sample. On the other hand, as the channel size increases, Young's modulus and yield strength are considerably reduced. The main conclusion is that parts with two scales of porosity can be designed by the 3D printing extrusion process.
如今,由于疾病和事故等各种问题,金属骨替代物的需求很高。因此,骨植入物被制造出具有定制的性能和微观结构,以便在人体中长期使用。为了改进此类植入物,3D打印是最有前景的技术。因此,这项工作旨在评估通过Ti6Al4V的挤出3D打印制造多孔材料。圆柱形样品由用于Ti6Al4V粉末金属注射成型的颗粒制成,形成具有三种不同尺寸的六边形通道。通过热膨胀测试评估致密化动力学,这使得能够跟踪样品在烧结循环期间的致密化过程。随后,通过扫描电子显微镜和X射线计算机断层扫描对样品进行表征,以分析其微观结构。压缩测试评估了烧结样品的机械强度。结果发现,随着通道尺寸的增加,打印过程中的六边形形状定义得更好。结果表明,在烧结过程中,每种通道尺寸都表现出类似的行为;然而,随着通道尺寸的减小,致密化程度更高。此外,在颗粒水平上获得了微孔,这些微孔完全相互连通,确保了流体在整个样品中的通过。另一方面,随着通道尺寸的增加,杨氏模量和屈服强度会显著降低。主要结论是,可以通过3D打印挤出工艺设计具有两种孔隙率尺度的部件。