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用于通过原子吸收光谱法测定七种元素的动物组织简单自动湿消化法。

Simple automated wet digestion of animal tissues for determination of seven elements by atomic absorption spectroscopy.

作者信息

Salisbury C D, Chan W

出版信息

J Assoc Off Anal Chem. 1985 Mar-Apr;68(2):218-9.

PMID:3988699
Abstract

A simple, automated wet digestion procedure was developed for the quantitative determination by atomic absorption spectroscopy (AAS) of arsenic, cadmium, copper, mercury, lead, selenium, and zinc in animal tissue. A commercial digestion block system with automated temperature programming was used. Recoveries of all elements from spiked bovine liver and kidney samples exceed 95%. The analytical results obtained for samples of NBS Bovine Liver (No. 1577a) agree well with certified values. The procedure is safe and requires minimum analyst time.

摘要

开发了一种简单的自动湿式消解程序,用于通过原子吸收光谱法(AAS)定量测定动物组织中的砷、镉、铜、汞、铅、硒和锌。使用了具有自动温度编程功能的商用消解块系统。加标牛肝和肾样品中所有元素的回收率均超过95%。对NBS牛肝(编号1577a)样品获得的分析结果与认证值吻合良好。该程序安全且所需分析人员时间最少。

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