Palacios Blanca, Mohammed Sohail M A K, Paul Tanaji, Garino Gia, Maribona Carlos, Langan Sean, Agarwal Arvind
Cold Spray and Rapid Advanced Deposition Laboratory, Department of Mechanical and Materials Engineering, Florida International University, 10555 West Flagler Street, Miami, FL 33174, USA.
Department of Materials Science and Engineering, Cornell University, Ithaca, NY 14850, USA.
Materials (Basel). 2025 Feb 6;18(3):724. doi: 10.3390/ma18030724.
This study investigates the scratch response of α-phase commercially pure titanium (cp-Ti) produced via wire arc directed energy deposition (WDED), focusing on the thermal history and directional effects. Progressive scratch tests (1-50 N) revealed heterogeneous wear properties between the top and bottom layers, with the top layer exhibiting higher material recovery (58 ± 5%) and wear volume (5.02 × 10 mm) compared to the bottom layer (42 ± 5% recovery, 4.46 × 10 mm), attributed to slower cooling rates and coarser grains enhancing ductility. The variation in the properties stems from the thermal gradient generated during WDED. Electron backscatter diffraction analysis showed higher kernel average misorientation (KAM) in the bottom layer (0.84° ± 0.49° vs. 0.51° ± 0.44°), affecting plasticity by reducing dislocation and twin boundary mobility. No significant differences were observed between longitudinal and transverse orientations, with coefficients of friction averaging 0.80 ± 0.12 and 0.79 ± 0.13, respectively. Abrasive wear dominated as the primary mechanism, accompanied by subsurface plastic deformation. These findings highlight the significant influence of WDED thermal history in governing scratch resistance and deformation behavior, providing valuable insights for optimizing cp-Ti components for high-performance applications.
本研究调查了通过电弧定向能量沉积(WDED)生产的α相商业纯钛(cp-Ti)的划痕响应,重点关注热历史和方向效应。渐进式划痕试验(1-50 N)揭示了顶层和底层之间的磨损特性不均匀,与底层(42±5%的恢复率,4.46×10 mm)相比,顶层表现出更高的材料恢复率(58±5%)和磨损体积(5.02×10 mm),这归因于较慢的冷却速率和更粗大的晶粒增强了延展性。性能的变化源于WDED过程中产生的热梯度。电子背散射衍射分析表明,底层的内核平均取向差(KAM)更高(0.84°±0.49°对0.51°±0.44°),通过降低位错和孪晶界迁移率影响塑性。纵向和横向取向之间未观察到显著差异,摩擦系数平均分别为0.80±0.12和0.79±0.13。磨粒磨损是主要机制,伴有亚表面塑性变形。这些发现凸显了WDED热历史对耐划痕性和变形行为的重大影响,为优化用于高性能应用的cp-Ti部件提供了有价值的见解。