Swain A R, Dutton S P, Truswell A S
J Am Diet Assoc. 1985 Aug;85(8):950-60.
To determine salicylate content, 333 food items were analyzed. Foods were homogenized with 25% sodium hydroxide, allowed to stand overnight, acidified with concentrated hydrochloric acid, and then extracted with warm diethylether over 5 hours. The extract was dried and taken up in dilute sodium bicarbonate solution for analysis. Salicylic acid was separated by high performance liquid chromatography and quantified by reading at 235 nm. Salicylic acid standards were used throughout to standardize extractions and analyses. This is the most comprehensive set of data on food salicylates yet published; extraction appears to have been more complete for some foods, giving higher values than those previously published. Most fruits, especially berry fruits and dried fruits, contain salicylate. Vegetables show a wide range from 0 to 6 mg salicylate per 100 gm food (for gherkins). Some herbs and spices were found to contain very high amounts per 100 gm, e.g., curry powder, paprika, thyme, garam masala, and rosemary. Among beverages, tea provides substantial amounts of salicylate. Licorice and peppermint candies and some honeys contain salicylates. Cereals, meat, fish, and dairy products contain none or negligible amounts.
为测定水杨酸盐含量,对333种食品进行了分析。将食品与25%的氢氧化钠匀浆,放置过夜,用浓盐酸酸化,然后用温热的乙醚萃取5小时。提取物经干燥后,用稀碳酸氢钠溶液溶解以供分析。水杨酸通过高效液相色谱法分离,并在235nm处进行读数定量。整个过程使用水杨酸标准品来标准化萃取和分析。这是迄今已发表的关于食品中水杨酸盐最全面的数据集;对于某些食品,萃取似乎更完全,得出的值高于先前发表的值。大多数水果,尤其是浆果类水果和干果,都含有水杨酸盐。蔬菜的水杨酸盐含量范围很广,每100克食品中为0至6毫克(如小黄瓜)。发现一些草药和香料每100克含有非常高的量,例如咖喱粉、辣椒粉、百里香、咖喱调料和迷迭香。在饮料中,茶含有大量的水杨酸盐。甘草和薄荷糖以及一些蜂蜜含有水杨酸盐。谷物、肉类、鱼类和乳制品不含或含有可忽略不计的量。